2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:917985-54-7
Molecular Formula:C16H27BO2S
Molecular Weight:294.266
Hs Code.:29349990
Mol file:917985-54-7.mol

Synonyms:2-(5-hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-di-oxaborolane;2-(5-HEXYL-2-THIENYL)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE;5-Hexyl-2-thiopheneboronic acid pinacol ester;2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-hexylthiophene;hexylthiophene boronic acid pinacol ester;

Suppliers and Price of 2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(5-Hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
100mg
$ 60.00

Sigma-Aldrich
5-Hexyl-2-thiopheneboronic acid pinacol ester 97%
5g
$ 499.00

Sigma-Aldrich
5-Hexyl-2-thiopheneboronic acid pinacol ester 97%
1g
$ 129.00

Crysdot
2-(5-Hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
1g
$ 202.00

Crysdot
2-(5-Hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
5g
$ 445.00

AOBChem
5-Hexylthiopheneboronicacidpinacolester 97%
25g
$ 943.00

American Custom Chemicals Corporation
5-HEXYL-2-THIOPHENEBORONIC ACID PINACOL ESTER 95.00%
1G
$ 405.30

American Custom Chemicals Corporation
5-HEXYL-2-THIOPHENEBORONIC ACID PINACOL ESTER 95.00%
5G
$ 1107.84

Ambeed
2-(5-Hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
5g
$ 561.00

Ambeed
2-(5-Hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 95+%
1g
$ 170.00

Total 29 raw suppliers

Chemical Property of 2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Refractive Index:n20/D 1.5
Boiling Point:140-142oC/0.5 mmHg
PSA：46.70000
Density:0.977 g/mL at 25oC
LogP:4.17010
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(5-Hexylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 7 articles about 2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 211737-28-9
2-bromo-5-hexylthiophene

: 917985-54-7
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-hexylthiophene

Guidance literature:: 2-bromo-5-hexylthiophene; With n-butyllithium; In tetrahydrofuran; at -70 ℃; for 0.75h;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at 25 ℃; for 18h;
DOI:10.1002/anie.201104275

Reference yield: 98.0%

: 18794-77-9
2-hexylthiophene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 917985-54-7
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-hexylthiophene

Guidance literature:: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In hexane; at 20 ℃; for 0.0833333h; Inert atmosphere;

2-hexylthiophene; In hexane; at 50 ℃; Inert atmosphere;
DOI:10.1002/anie.201004055

Reference yield: 87.0%

: 18794-77-9
2-hexylthiophene

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 917985-54-7
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-5-hexylthiophene

Guidance literature:: 2-hexylthiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1021/acs.inorgchem.6b00842