(E)-N-(3-Bromopropyl)-1-(2,3,4-trimethoxyphenyl)methanimine

Base Information

• Chemical Name: (E)-N-(3-Bromopropyl)-1-(2,3,4-trimethoxyphenyl)methanimine
• CAS No.: 918335-87-2
• Molecular Formula: C₁₃H₁₈BrNO₃
• Molecular Weight: 316.195
• DSSTox Substance ID: DTXSID30582662
• Mol file: 918335-87-2.mol

Synonyms:918335-87-2;(E)-N-(3-Bromopropyl)-1-(2,3,4-trimethoxyphenyl)methanimine;DTXSID30582662;1-Propanamine,3-bromo-N-[(2,3,4-trimethoxyphenyl)methylene]-

Chemical Property of (E)-N-(3-Bromopropyl)-1-(2,3,4-trimethoxyphenyl)methanimine

Chemical Property:

• Vapor Pressure: 6.44E-06mmHg at 25°C
• Boiling Point: 389.3oC at 760 mmHg
• Flash Point: 189.3oC
• PSA: 40.05000
• Density: 1.27g/cm3
• LogP: 2.91630
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 315.04701
• Heavy Atom Count: 18
• Complexity: 250

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C(=C(C=C1)C=NCCCBr)OC)OC

Technology Process of (E)-N-(3-Bromopropyl)-1-(2,3,4-trimethoxyphenyl)methanimine

There total 2 articles about (E)-N-(3-Bromopropyl)-1-(2,3,4-trimethoxyphenyl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-bromopropylamine hydrochloride (5003-71-4) + 2,3,4-trimethoxybenzaldehyde (2103-57-3) → 2,3,4-trimethoxybenzylidene-(3-bromo-1-propylamine) (918335-87-2)

Guidance literature:

3-bromopropylamine hydrochloride; With triethylamine; In chloroform; at 20 ℃; for 0.0833333h;

2,3,4-trimethoxybenzaldehyde; With magnesium sulfate; In chloroform; at 20 ℃; for 16h;

DOI:10.1021/jm060974n

Reference yield:

3-bromopropylamine hydrochloride (5003-71-4) + 2,3,4-trimethoxybenzaldehyde (2103-57-3) → C13H18BrNO3 (918335-87-2)

Guidance literature:

With magnesium sulfate; triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1055/s-0033-1338647

upstream raw materials:

3-bromopropylamine hydrochloride

2,3,4-trimethoxybenzaldehyde