Methyl 14-[4-(4-methylbenzoyl)phenyl]tetradecanoate

Base Information

Chemical Name:Methyl 14-[4-(4-methylbenzoyl)phenyl]tetradecanoate
CAS No.:918500-21-7
Molecular Formula:C29H40O3
Molecular Weight:436.635
Hs Code.:
DSSTox Substance ID:DTXSID30582602
Wikidata:Q82474072

Synonyms:918500-21-7;METHYL 14-[4-(4-METHYLBENZOYL)PHENYL]TETRADECANOATE;DTXSID30582602

Suppliers and Price of Methyl 14-[4-(4-methylbenzoyl)phenyl]tetradecanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 14-[4-(4-methylbenzoyl)phenyl]tetradecanoate

Chemical Property:

XLogP3:9.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:17
Exact Mass:436.29774513
Heavy Atom Count:32
Complexity:499

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C2=CC=C(C=C2)CCCCCCCCCCCCCC(=O)OC

Technology Process of Methyl 14-[4-(4-methylbenzoyl)phenyl]tetradecanoate

There total 5 articles about Methyl 14-[4-(4-methylbenzoyl)phenyl]tetradecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76693-57-7
(4-bromophenyl)(p-tolyl)methanone

: 54716-25-5
13-tetradecenoic acid methyl ester

: 918500-21-7
methyl 14-(4-(4-methylbenzoyl)phenyl)tetradecanoate

Guidance literature:: 13-tetradecenoic acid methyl ester; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 4h;

(4-bromophenyl)(p-tolyl)methanone; With triphenyl-arsane; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; water; N,N-dimethyl-formamide; Heating;
DOI:10.1021/jo061617n

Reference yield:

: 7331-03-5
13-tetradecenoic acid

: 918500-21-7
methyl 14-(4-(4-methylbenzoyl)phenyl)tetradecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / H₂SO₄ / Heating

2.1: 9-BBN / tetrahydrofuran / 4 h / 20 °C

2.2: 2.15 g / Cs₂CO₃; AsPh₃ / Pd(dppf)Cl₂ / tetrahydrofuran; dimethylformamide; H₂O / Heating

With 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; In tetrahydrofuran; 2.2: Suzuki coupling;
DOI:10.1021/jo061617n

Reference yield:

: 7766-50-9
1-undecen-11-ylbromide

: 918500-21-7
methyl 14-(4-(4-methylbenzoyl)phenyl)tetradecanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / 2 h / 45 °C

1.2: 82 percent / CuCl / tetrahydrofuran / 1 h / 0 °C

2.1: 98 percent / H₂SO₄ / Heating

3.1: 9-BBN / tetrahydrofuran / 4 h / 20 °C

3.2: 2.15 g / Cs₂CO₃; AsPh₃ / Pd(dppf)Cl₂ / tetrahydrofuran; dimethylformamide; H₂O / Heating

With 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; magnesium; In tetrahydrofuran; 3.2: Suzuki coupling;
DOI:10.1021/jo061617n