Technology Process of Pentadecanoic acid, 15-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]-, methyl
ester
There total 9 articles about Pentadecanoic acid, 15-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]-, methyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium molybdate tetrahydrate; dihydrogen peroxide;
In
tetrahydrofuran;
at 15 - 20 ℃;
DOI:10.1016/j.tet.2006.09.019
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 81 percent / hydrogen peroxide; ammonium heptamolybdate(VI) tetrahydrate / tetrahydrofuran; various solvent(s) / 20 °C
2: 80 percent / lithium hexamethyldisilazide / tetrahydrofuran / -10 - 20 °C
3: 92 percent / hydrogen / palladium on carbon / methanol; tetrahydrofuran
4: 91 percent / anhydrous potassium carbonate / acetone / 16 h / 20 °C
5: 91 percent / hydrogen peroxide; ammonium heptamolybdate(VI) tetrahydrate / tetrahydrofuran; various solvent(s) / 15 - 20 °C
With
ammonium molybdate tetrahydrate; hydrogen; dihydrogen peroxide; potassium carbonate; lithium hexamethyldisilazane;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; acetone;
2: Kocienski-Julia reaction;
DOI:10.1016/j.tet.2006.09.019
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / lithium hexamethyldisilazide / tetrahydrofuran / -10 - 20 °C
2: 92 percent / hydrogen / palladium on carbon / methanol; tetrahydrofuran
3: 91 percent / anhydrous potassium carbonate / acetone / 16 h / 20 °C
4: 91 percent / hydrogen peroxide; ammonium heptamolybdate(VI) tetrahydrate / tetrahydrofuran; various solvent(s) / 15 - 20 °C
With
ammonium molybdate tetrahydrate; hydrogen; dihydrogen peroxide; potassium carbonate; lithium hexamethyldisilazane;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; acetone;
1: Kocienski-Julia reaction;
DOI:10.1016/j.tet.2006.09.019
