L-Tyrosine, N-[[[2-[(2-aminoacetyl)amino]ethyl][(1,1-dimethylethoxy)carbonyl]amino] [[(1,1-dimethylethoxy)carbonyl]amino]methylene]-, methyl ester

Base Information

Chemical Name:L-Tyrosine, N-[[[2-[(2-aminoacetyl)amino]ethyl][(1,1-dimethylethoxy)carbonyl]amino] [[(1,1-dimethylethoxy)carbonyl]amino]methylene]-, methyl ester
CAS No.:918956-21-5
Molecular Formula:C₂₅H₃₉N₅O₈
Molecular Weight:537.613
Hs Code.:

L-Tyrosine,
N-[[[2-[(2-aminoacetyl)amino]ethyl][(1,1-dimethylethoxy)carbonyl]amino]
[[(1,1-dimethylethoxy)carbonyl]amino]methylene]-, methyl ester

Synonyms:

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Chemical Property of L-Tyrosine, N-[[[2-[(2-aminoacetyl)amino]ethyl][(1,1-dimethylethoxy)carbonyl]amino] [[(1,1-dimethylethoxy)carbonyl]amino]methylene]-, methyl ester

Chemical Property:

Purity/Quality:

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Hazard Codes:

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Technology Process of L-Tyrosine, N-[[[2-[(2-aminoacetyl)amino]ethyl][(1,1-dimethylethoxy)carbonyl]amino] [[(1,1-dimethylethoxy)carbonyl]amino]methylene]-, methyl ester

There total 4 articles about L-Tyrosine, N-[[[2-[(2-aminoacetyl)amino]ethyl][(1,1-dimethylethoxy)carbonyl]amino] [[(1,1-dimethylethoxy)carbonyl]amino]methylene]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 918956-20-4
(S)-2-(N',N''-di(tert-butoxycarbonyl)-N'-{2-[2-(9H-fluoren-9-ylmethoxycarbonylamino)acetylamino]ethyl}guanidino)-3-(4-hydroxyphenyl)propionic acid methyl ester

: 918956-21-5
C₂₅H₃₉N₅O₈

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1002/chem.200600366

Reference yield:

: [2-(1,3-di(tert-butoxycarbonyl)-2-methylisothioureido)ethyl]carbamic acid allyl ester

: 918956-21-5
C₂₅H₃₉N₅O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: 56 percent / tetrahydrofuran / 15 h / Heating

2.1: DIC; HOBt / CH₂Cl₂ / 0.5 h / 20 °C

2.2: 67 percent / tributyltin hydride / Pd(PPh₃)4 / CH₂Cl₂ / 12 h / 20 °C

3.1: piperidine / dimethylformamide / 1 h / 20 °C

With piperidine; benzotriazol-1-ol; dacarbazine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600366

Reference yield:

: 918956-16-8
(S)-2-[N'-(2-allyloxycarbonylaminoethyl)-N',N''-di(tert-butoxycarbonyl)guanidino]-3-(4-hydroxyphenyl)propionic acid methyl ester

: 918956-21-5
C₂₅H₃₉N₅O₈

Guidance literature:: Multi-step reaction with 2 steps

1.1: DIC; HOBt / CH₂Cl₂ / 0.5 h / 20 °C

1.2: 67 percent / tributyltin hydride / Pd(PPh₃)4 / CH₂Cl₂ / 12 h / 20 °C

2.1: piperidine / dimethylformamide / 1 h / 20 °C

With piperidine; benzotriazol-1-ol; dacarbazine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600366