1,2,4-Trimethylphenanthrene

Base Information

Chemical Name:1,2,4-Trimethylphenanthrene
CAS No.:23189-64-2
Molecular Formula:C₁₇H₁₆
Molecular Weight:220.314
Hs Code.:2902909090
DSSTox Substance ID:DTXSID20177763
Nikkaji Number:J1.610.667D
Wikidata:Q83048099
Mol file:23189-64-2.mol

Synonyms:1,2,4-TRIMETHYLPHENANTHRENE;23189-64-2;Phenanthrene,1,2,4-trimethyl-;DTXSID20177763;Phenanthrene, 1,2,4-trimethyl-

Suppliers and Price of 1,2,4-Trimethylphenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2,4-TMP 95.00%
5MG
$ 496.21

Total 3 raw suppliers

Chemical Property of 1,2,4-Trimethylphenanthrene

Chemical Property:

Vapor Pressure:7.25E-06mmHg at 25°C
Boiling Point:387.6°C at 760 mmHg
Flash Point:180.3°C
PSA：0.00000
Density:1.066g/cm³
LogP:4.91820
XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:220.125200510
Heavy Atom Count:17
Complexity:269

Purity/Quality:

99% ^*data from raw suppliers

1,2,4-TMP 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C2C(=C1C)C=CC3=CC=CC=C32)C

Technology Process of 1,2,4-Trimethylphenanthrene

There total 12 articles about 1,2,4-Trimethylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74569-47-4
7-methoxy-1,1,4a-trimethyl-3,4,4a,9-tetrahydro-1H-phenanthren-2-one

: 23189-64-2
1,2,4-Trimethyl-phenanthren

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / p-toluolsulphonic acid, acetic acid / 70 h / Heating

2: BBr₃ / CH₂Cl₂ / 1 h / -25 °C

3: NaBH₄, CF₃CO₂H / CH₂Cl₂ / 28 h / 0 °C

With sodium tetrahydroborate; boron tribromide; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)96118-6

Reference yield:

: 134219-83-3
5,7,8-Trimethyl-phenanthren-2-ol

: 23189-64-2
1,2,4-Trimethyl-phenanthren

Guidance literature:: With sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 28h; Yield given;
DOI:10.1016/S0040-4020(01)96118-6

Reference yield:

: 134219-81-1
7-Methoxy-1,2,4-trimethyl-9,10-dihydro-phenanthrene

: 23189-64-2
1,2,4-Trimethyl-phenanthren

Guidance literature:: Multi-step reaction with 3 steps

1: 12 mg / Pd/charcoal / 0.67 h / Heating; metal bath

2: BBr₃ / CH₂Cl₂ / 1 h / -25 °C

3: NaBH₄, CF₃CO₂H / CH₂Cl₂ / 28 h / 0 °C

With sodium tetrahydroborate; boron tribromide; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane;
DOI:10.1016/S0040-4020(01)96118-6