Dibenz[a,j]anthracene-3,4-diol, 3,4-dihydro-, trans-

Base Information

Chemical Name:Dibenz[a,j]anthracene-3,4-diol, 3,4-dihydro-, trans-
CAS No.:119053-18-8
Molecular Formula:C26H20O4
Molecular Weight:0
Hs Code.:
Mol file:119053-18-8.mol

Synonyms:3,4-Dihydrodihydroxydibenz(a,j)anthracene;3,4-Ddda;Dibenz(a,j)anthracene-3,4-dihydrodiol;Dibenz(a,j)anthracene-3,4-diol, 3,4-dihydro-, trans-;3,4-Dihydrodioldibenz(a,j)anthracene;

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Chemical Property of Dibenz[a,j]anthracene-3,4-diol, 3,4-dihydro-, trans-

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Technology Process of Dibenz[a,j]anthracene-3,4-diol, 3,4-dihydro-, trans-

There total 6 articles about Dibenz[a,j]anthracene-3,4-diol, 3,4-dihydro-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 114326-32-8,137766-02-0
(-)-(3R,4R)-trans-3,4-dihydrodibenzanthracen-3,4-diyl diacetate

: 88190-96-9,114326-33-9,119053-18-8,137766-09-7
(-)-(3R,4R)-trans-3,4-dihydrodibenzanthracen-3,4-diol

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; for 18h; Ambient temperature;

Reference yield:

: 137676-25-6
(-)-(3R,4S)-3,4-epoxy-1,2,3,4-tetrahydrodibenzanthracene

: 88190-96-9,114326-33-9,119053-18-8,137766-09-7
(-)-(3R,4R)-trans-3,4-dihydrodibenzanthracen-3,4-diol

Guidance literature:: Multi-step reaction with 5 steps

1: 38 percent / water / dioxane / 0.5 h / pH 2.5 (perchloric acid, sodium perchlorate)

2: 62 percent / p-dimethylaminopyridine, pyridine / 0.5 h

3: 85 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 0.33 h / 75 °C

4: 28 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / tetrahydrofuran / 16 h / Ambient temperature

5: 58 percent / ammonia / tetrahydrofuran; methanol / 18 h / Ambient temperature

With pyridine; dmap; N-Bromosuccinimide; azobisisobutyronitrile; DBN; ammonia; water; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane;

Reference yield:

: 137676-27-8
(-)-(3R,4R)-trans-1,2,3,4-tetrahydrodibenzanthracen-3,4-diyl diacetate

: 88190-96-9,114326-33-9,119053-18-8,137766-09-7
(-)-(3R,4R)-trans-3,4-dihydrodibenzanthracen-3,4-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 0.33 h / 75 °C

2: 28 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / tetrahydrofuran / 16 h / Ambient temperature

3: 58 percent / ammonia / tetrahydrofuran; methanol / 18 h / Ambient temperature

With N-Bromosuccinimide; azobisisobutyronitrile; DBN; ammonia; In tetrahydrofuran; methanol; tetrachloromethane;