â-D-Glucopyranoside,4-(2-propenyl)phenyl 6-O-â-D-xylopyranosyl-

Base Information

Chemical Name:â-D-Glucopyranoside,4-(2-propenyl)phenyl 6-O-â-D-xylopyranosyl-
CAS No.:66648-51-9
Molecular Formula:C₂₀H₂₈O₁₀
Molecular Weight:428.436
Hs Code.:

Synonyms:

Suppliers and Price of â-D-Glucopyranoside,4-(2-propenyl)phenyl 6-O-â-D-xylopyranosyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of â-D-Glucopyranoside,4-(2-propenyl)phenyl 6-O-â-D-xylopyranosyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of â-D-Glucopyranoside,4-(2-propenyl)phenyl 6-O-â-D-xylopyranosyl-

There total 9 articles about â-D-Glucopyranoside,4-(2-propenyl)phenyl 6-O-â-D-xylopyranosyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 95058-14-3
miyaginin hexaacetate

: 66648-51-9
miyaginin

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1246/bcsj.57.2893

Reference yield:

: 501-92-8
4-(prop-2-enyl)phenol

: 66648-51-9
miyaginin

Guidance literature:: Multi-step reaction with 7 steps

1: 56 percent / acetic anhydride, p-toluenesulfonic acid / 0.83 h / 100 - 110 °C / 20 Torr

2: 84 percent / CH₃ONa / methanol / 2 h / Ambient temperature

3: pyridine / 7 h / 100 °C

4: pyridine / 4.5 h / Ambient temperature

5: 80percent aq. CH₃CO₂H / 100 deg C, 30 min, room temperature

6: 88 percent / HgBr₂, Hg(CN)2 / acetonitrile / 5 h / Ambient temperature

7: 89 percent / CH₃ONa / methanol

With pyridine; sodium methylate; mercury(II) cyanide; acetic anhydride; toluene-4-sulfonic acid; acetic acid; mercury dibromide; In methanol; acetonitrile;
DOI:10.1246/bcsj.57.2893

Reference yield:

: 10210-17-0
3-(4-hydroxyphenyl)propan-1-ol

: 66648-51-9
miyaginin

Guidance literature:: Multi-step reaction with 9 steps

1: 100 percent / tributylphosphine / tetrahydrofuran / 5 h / Ambient temperature

2: 80 percent / 30percent aq. H₂O₂ / tetrahydrofuran / 3.5 h / 40 °C

3: 56 percent / acetic anhydride, p-toluenesulfonic acid / 0.83 h / 100 - 110 °C / 20 Torr

4: 84 percent / CH₃ONa / methanol / 2 h / Ambient temperature

5: pyridine / 7 h / 100 °C

6: pyridine / 4.5 h / Ambient temperature

7: 80percent aq. CH₃CO₂H / 100 deg C, 30 min, room temperature

8: 88 percent / HgBr₂, Hg(CN)2 / acetonitrile / 5 h / Ambient temperature

9: 89 percent / CH₃ONa / methanol

With pyridine; tributylphosphine; dihydrogen peroxide; sodium methylate; mercury(II) cyanide; acetic anhydride; toluene-4-sulfonic acid; acetic acid; mercury dibromide; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1246/bcsj.57.2893