Methyl 3-(acetylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Base Information

Chemical Name:Methyl 3-(acetylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside
CAS No.:17016-62-5
Molecular Formula:C₉H₁₇NO₄
Molecular Weight:203.238
Hs Code.:

Synonyms:D-arabino-Hexopyranoside,methyl 3-acetamido-2,3,6-trideoxy-, a- (8CI); NSC 276417

Suppliers and Price of Methyl 3-(acetylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of Methyl 3-(acetylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside

Chemical Property:

Vapor Pressure:2.73E-08mmHg at 25°C
Boiling Point:406.2°Cat760mmHg
PKA:13.59±0.70(Predicted)
Flash Point:199.5°C
PSA：67.79000
Density:1.15g/cm³
LogP:0.02420

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methyl 3-(acetylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside

There total 18 articles about Methyl 3-(acetylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2,3,4,6-tetradeoxy-4',5'-dihydro-2'-methyl(methyl α-DL-lyxo-hexopyranosido)<3,4-d>oxazole

: 6605-27-2,17016-62-5,23089-57-8,23089-61-4,32385-07-2,40879-86-5,53626-04-3,57918-56-6,58769-78-1,67693-35-0,67776-31-2,73979-08-5,91517-12-3,91752-71-5,91752-72-6,93253-07-7,93274-51-2,103773-72-4
methyl 3-acetamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside

Guidance literature:: With pyridine; toluene-4-sulfonic acid; In water; at 100 ℃; for 2h;

Reference yield:

: 96796-64-4
methyl 2,6-dideoxy-4-O-methoxymethyl-α-L-ribo-hexopyranoside

: 6605-27-2,17016-62-5,23089-57-8,23089-61-4,32385-07-2,40879-86-5,53626-04-3,57918-56-6,58769-78-1,67693-35-0,67776-31-2,73979-08-5,91517-12-3,91752-71-5,91752-72-6,93253-07-7,93274-51-2,103773-72-4
methyl 3-acetamido-2,3,6-trideoxy-β-L-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / pyridine / Ambient temperature

2: 69 percent / NaN₃ / dimethylformamide / 100 °C / overnight

3: 96 percent / H₂ / platinum(IV) oxide / methanol / Ambient temperature; under slight overpressure

4: 1.5 M HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; sodium azide; hydrogen; platinum(IV) oxide; In pyridine; methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(85)85215-0

Reference yield:

: 96796-66-6
methyl 3-azido-2,3,6-trideoxy-4-O-methoxymethyl-α-L-arabino-hexopyranoside

: 6605-27-2,17016-62-5,23089-57-8,23089-61-4,32385-07-2,40879-86-5,53626-04-3,57918-56-6,58769-78-1,67693-35-0,67776-31-2,73979-08-5,91517-12-3,91752-71-5,91752-72-6,93253-07-7,93274-51-2,103773-72-4
methyl 3-acetamido-2,3,6-trideoxy-β-L-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂ / platinum(IV) oxide / methanol / Ambient temperature; under slight overpressure

2: 1.5 M HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; hydrogen; platinum(IV) oxide; In methanol;
DOI:10.1016/0008-6215(85)85215-0