1H-Benzimidazole-1-carboxylic acid, 7-[1-[(1,1-dimethylethoxy)carbonyl]-1H-pyrrol-3-yl]-2,3-dihydro-2-oxo-3-( phenylmethyl)-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: 1H-Benzimidazole-1-carboxylic acid, 7-[1-[(1,1-dimethylethoxy)carbonyl]-1H-pyrrol-3-yl]-2,3-dihydro-2-oxo-3-( phenylmethyl)-, 1,1-dimethylethyl ester
• CAS No.: 920285-25-2
• Molecular Formula: C28H31N3O5
• Molecular Weight: 489.571

Synonyms:

Chemical Property of 1H-Benzimidazole-1-carboxylic acid, 7-[1-[(1,1-dimethylethoxy)carbonyl]-1H-pyrrol-3-yl]-2,3-dihydro-2-oxo-3-( phenylmethyl)-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Benzimidazole-1-carboxylic acid, 7-[1-[(1,1-dimethylethoxy)carbonyl]-1H-pyrrol-3-yl]-2,3-dihydro-2-oxo-3-( phenylmethyl)-, 1,1-dimethylethyl ester

There total 1 articles about 1H-Benzimidazole-1-carboxylic acid, 7-[1-[(1,1-dimethylethoxy)carbonyl]-1H-pyrrol-3-yl]-2,3-dihydro-2-oxo-3-( phenylmethyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzyl-2-oxo-7-(1H-pyrrol-3-yl)-2,3-dihydro-benzoimidazole-1-carboxylic acid tert-butyl ester (920285-26-3) + di-tert-butyl dicarbonate (24424-99-5) → 3-benzyl-7-(1-tert-butoxycarbonyl-1H-pyrrol-3-yl)-2-oxo-2,3-dihydro-benzoimidazole-1-carboxylic acid tert-butyl ester (920285-25-2)

Guidance literature:

With dmap; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

3-benzyl-7-(1-tert-butoxycarbonyl-1H-pyrrol-3-yl)-2-oxo-2,3-dihydro-benzoimidazole-1-carboxylic acid tert-butyl ester (920285-25-2) → 3-benzyl-7-(1-tert-butoxycarbonyl-pyrrolidin-3-yl)-2-oxo-2,3-dihydro-benzoimidazole-1-carboxylic acid tert-butyl ester (920285-27-4)

Guidance literature:

With hydrogen; platinum on carbon; In methanol; for 95h; under 760.051 Torr;

upstream raw materials:

3-benzyl-2-oxo-7-(1H-pyrrol-3-yl)-2,3-dihydro-benzoimidazole-1-carboxylic acid tert-butyl ester

di-tert-butyl dicarbonate

Downstream raw materials:

3-benzyl-7-(1-tert-butoxycarbonyl-pyrrolidin-3-yl)-2-oxo-2,3-dihydro-benzoimidazole-1-carboxylic acid tert-butyl ester

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