decan-3-amine

Base Information

• Chemical Name: decan-3-amine
• CAS No.: 4088-36-2
• Molecular Formula: C10H23 N
• Molecular Weight: 157.2963
• Hs Code.: 2921199090
• Mol file: 4088-36-2.mol

Synonyms:Octylamine,N-ethyl- (6CI,7CI,8CI); Ethyloctylamine; N-Ethyl-1-octanamine

Chemical Property of decan-3-amine

Chemical Property:

• Vapor Pressure: 0.185mmHg at 25°C
• Melting Point: -38.5°C (estimate)
• Refractive Index: 1.4286
• Boiling Point: 211.2 °C at 760 mmHg
• PKA: 10.93±0.19(Predicted)
• Flash Point: 81.8 °C
• PSA: 26.02000
• Density: 0.795 g/cm³
• LogP: 3.78450

Purity/Quality:

98%min ^*data from raw suppliers

ETHYL(OCTYL)AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of decan-3-amine

There total 6 articles about decan-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

triethyl borane (97-94-9) + N-chloro-1-octylamine (89231-76-5) → ethyl-n-octylamine (4088-36-2)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

DOI:10.1021/jo00183a035

Reference yield:

N-octylacetamide (7462-62-6) → ethyl-n-octylamine (4088-36-2)

Guidance literature:

With phenylsilane-d3; C₃₆H₄₈F₆N₆NiO₅S₂; In toluene; at 110 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1039/d1cc03537a

Reference yield:

n-Octylamine (111-86-4) → ethyl-n-octylamine (4088-36-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: C₃₆H₄₈F₆N₆NiO₅S₂; phenylsilane-d3 / toluene / 24 h / 110 °C / Inert atmosphere; Schlenk technique

With phenylsilane-d3; C₃₆H₄₈F₆N₆NiO₅S₂; triethylamine; In dichloromethane; toluene;

DOI:10.1039/d1cc03537a

upstream raw materials:

N-ethyl-N-octyl-toluene-4-sulfonamide

triethyl borane

N-chloro-1-octylamine

n-Octylamine

Refernces

• 1、 Klamann,Hofbauer. "-". . p. 62,75. Retrieved 1953.