2-Thiophenecarboxamide, N-[4-[3-[(3-amino-1-oxopropyl)amino]phenyl]-6-(4-chloro-2-hydroxyphen yl)-3-cyano-2-pyridinyl]-, 2,2,2-trifluoroacetate (1:1)

Base Information

• Chemical Name: 2-Thiophenecarboxamide, N-[4-[3-[(3-amino-1-oxopropyl)amino]phenyl]-6-(4-chloro-2-hydroxyphen yl)-3-cyano-2-pyridinyl]-, 2,2,2-trifluoroacetate (1:1)
• CAS No.: 925924-95-4
• Molecular Formula: C₂HF₃O₂*C₂₆H₂₀ClN₅O₃S
• Molecular Weight: 632.019

Synonyms:

Chemical Property of 2-Thiophenecarboxamide, N-[4-[3-[(3-amino-1-oxopropyl)amino]phenyl]-6-(4-chloro-2-hydroxyphen yl)-3-cyano-2-pyridinyl]-, 2,2,2-trifluoroacetate (1:1)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Thiophenecarboxamide, N-[4-[3-[(3-amino-1-oxopropyl)amino]phenyl]-6-(4-chloro-2-hydroxyphen yl)-3-cyano-2-pyridinyl]-, 2,2,2-trifluoroacetate (1:1)

There total 1 articles about 2-Thiophenecarboxamide, N-[4-[3-[(3-amino-1-oxopropyl)amino]phenyl]-6-(4-chloro-2-hydroxyphen yl)-3-cyano-2-pyridinyl]-, 2,2,2-trifluoroacetate (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

tert-butyl {3-[(3-{6-[4-chloro-2-(methoxymethoxy)-phenyl]-3-cyano-2-[(thiophen-2-ylcarbonyl)amino]pyridin-4-yl}phenyl)amino]-3-oxopropyl}carbamate (925922-45-8) + trifluoroacetic acid (76-05-1) → N-{4-[3-(β-alanylamino)phenyl]-6-(4-chloro-2-hydroxy-phenyl)-3-cyanopyridin-2-yl}thiophene-2-carboxamide trifluoroacetate (925924-95-4)

Guidance literature:

at 20 ℃; for 1.5h;

DOI:10.1016/j.bmc.2010.04.036

upstream raw materials:

tert-butyl {3-[(3-{6-[4-chloro-2-(methoxymethoxy)-phenyl]-3-cyano-2-[(thiophen-2-ylcarbonyl)amino]pyridin-4-yl}phenyl)amino]-3-oxopropyl}carbamate

trifluoroacetic acid

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