1,10-Phenanthrolin-2(1H)-one

Base Information

Chemical Name:1,10-Phenanthrolin-2(1H)-one
CAS No.:92695-50-6
Molecular Formula:C12H8N2O
Molecular Weight:196.208
Hs Code.:
DSSTox Substance ID:DTXSID60469694
Nikkaji Number:J1.702.863D
Wikidata:Q82297518

Synonyms:1,10-Phenanthrolin-2(1H)-one;1H-1,10-phenanthrolin-2-one;92695-50-6;phenanthrolinone;hydroxyphenanthroline;SCHEMBL169928;DTXSID60469694;EN300-6495603

Suppliers and Price of 1,10-Phenanthrolin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,10-Phenanthrolin-2(1H)-one

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:196.063662883
Heavy Atom Count:15
Complexity:300

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C3=C(C=C2)C=CC(=O)N3)N=C1

Technology Process of 1,10-Phenanthrolin-2(1H)-one

There total 12 articles about 1,10-Phenanthrolin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: C₄₂H₃₀N₄O

: C₃₀H₂₄N₂O

: 92695-50-6
1H-[1,10]phenanthrolin-2-one

Guidance literature:: C₄₂H₃₀N₄O; With potassium tert-butylate; In toluene; at 125 ℃; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/acscatal.9b01145

Reference yield: 94.0%

: 2-(2,6-bis(phenylthio)phenoxy)-1,10-phenanthroline

: 68143-72-6
2,6-bis(phenylthio)phenol

: 92695-50-6
1H-[1,10]phenanthrolin-2-one

Guidance literature:: 2-(2,6-bis(phenylthio)phenoxy)-1,10-phenanthroline; With potassium tert-butylate; 1,3,5-trimethyl-benzene; at 160 ℃; for 19.5h; Sealed tube; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/acs.orglett.0c02012

Reference yield:

: 2-(1,10-phenanthrolyl) hydrogenphthalate

: 88-99-3,73607-73-5
benzene-1,2-dicarboxylic acid

: 92695-50-6
2-hydroxyl-1,10-phenanthroline

Guidance literature:: With potassium chloride; Cu(II) salt; In acetonitrile; at 30 ℃; pH=3.2; Further Variations:; pH-values; Catalysts; Kinetics;
DOI:10.1006/bioo.2000.1176