3,3',5,5'-Tetrachlorobenzophenone

Base Information

• Chemical Name: 3,3',5,5'-Tetrachlorobenzophenone
• CAS No.: 92758-86-6
• Molecular Formula: C₁₃H₆Cl₄O
• Molecular Weight: 320.002
• Hs Code.: 2914700090
• DSSTox Substance ID: DTXSID70384440
• Wikidata: Q82176583
• Mol file: 92758-86-6.mol

Synonyms:3,3',5,5'-Tetrachlorobenzophenone;92758-86-6;bis(3,5-dichlorophenyl)methanone;MFCD01763607;HMS549L10;CDS1_000604;Maybridge1_002892;DivK1c_001644;SCHEMBL4465360;DTXSID70384440;bis(2,4-dichlorophenyl)-methanone;bis-(3,5-dichloro-phenyl)-methanone;AKOS016018491;CCG-243860

Chemical Property of 3,3',5,5'-Tetrachlorobenzophenone

Chemical Property:

• Vapor Pressure: 4.85E-08mmHg at 25°C
• Boiling Point: 442.9oC at 760 mmHg
• Flash Point: 186.7oC
• PSA: 17.07000
• Density: 1.485g/cm3
• LogP: 5.53120
• XLogP3: 5.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 319.914325
• Heavy Atom Count: 18
• Complexity: 261

Purity/Quality:

98% ^*data from raw suppliers

3,3',5,5'-Tetrachlorobenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C=C(C=C1Cl)Cl)C(=O)C2=CC(=CC(=C2)Cl)Cl

Technology Process of 3,3',5,5'-Tetrachlorobenzophenone

There total 1 articles about 3,3',5,5'-Tetrachlorobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

→ bis(3,5-dichlorophenyl)methanone (92758-86-6)

Guidance literature:

With copper(l) iodide; 5% Pd-CaCO3; In dimethyl sulfoxide; at 50 ℃; for 12h; under 114.008 - 1406.09 Torr;

Reference yield: 86.0%

bis(3,5-dichlorophenyl)methanone (92758-86-6) + acetylenemagnesium bromide (4301-14-8) → 1,1-bis(3,5-dichlorophenyl)-2-propyn-1-ol

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c4nj02034k