3-(PHENOXYMETHYL)ANILINE

Base Information

• Chemical Name: 3-(PHENOXYMETHYL)ANILINE
• CAS No.: 93189-16-3
• Molecular Formula: C13H13NO
• Molecular Weight: 199.252
• Hs Code.: 2922299090
• Mol file: 93189-16-3.mol

Synonyms:Benzenamine,3-(bromomethyl);m-Amino-benzylbromid;3-(BROMOMETHYL)-ANILINE;3-(phenoxymethyl)-benzenamine;m-Amino-benzyl-O-phenylaether;

Chemical Property of 3-(PHENOXYMETHYL)ANILINE

Chemical Property:

• Vapor Pressure: 2.76E-05mmHg at 25°C
• Melting Point: 45 °C
• Boiling Point: 357℃
• Flash Point: 180℃
• PSA: 35.25000
• Density: 1.129
• LogP: 3.42900

Purity/Quality:

99%, ^*data from raw suppliers

3-(phenoxymethyl)aniline ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22-36/37/38
• Safety Statements: 22-26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(PHENOXYMETHYL)ANILINE

There total 5 articles about 3-(PHENOXYMETHYL)ANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-nitro-3-(phenoxymethyl)benzene (17414-84-5) → 3-(phenoxymethyl)aniline (93189-16-3)

Guidance literature:

With platinum(IV) oxide; hydrogen; In ethyl acetate; at 70 ℃; under 760.051 Torr; Flow reactor;

DOI:10.1021/acs.jmedchem.6b01018

Reference yield:

1-bromomethyl-3-nitrobenzene (3958-57-4) → 3-(phenoxymethyl)aniline (93189-16-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: iron; ammonium chloride / water; ethanol / 1 h

With iron; potassium carbonate; ammonium chloride; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2017.04.010

Reference yield:

phenol (108-95-2,27073-41-2) → 3-(phenoxymethyl)aniline (93189-16-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: iron; ammonium chloride / water; ethanol / 1 h

With iron; potassium carbonate; ammonium chloride; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2017.04.010

upstream raw materials:

bromobenzene

3-Nitrobenzyl alcohol

1-nitro-3-(phenoxymethyl)benzene

1-bromomethyl-3-nitrobenzene

Downstream raw materials:

3-(phenoxymethyl)phenyl isocyanate

N-(3-Phenoxymethyl-phenyl)-propionamide

5-(3-(phenoxymethyl)phenyl)-1H-tetrazole

3-azidobenzyl phenyl ether

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