(E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene

Base Information

Chemical Name:(E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene
CAS No.:93323-17-2
Molecular Formula:C17H14N2
Molecular Weight:246.312
Hs Code.:
DSSTox Substance ID:DTXSID30573353
Nikkaji Number:J1.287.286K

Synonyms:93323-17-2;(E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene;DTXSID30573353

Suppliers and Price of (E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:246.115698455
Heavy Atom Count:19
Complexity:304

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=NC2=C3C=CC=CC=C3C=C2

Technology Process of (E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene

There total 4 articles about (E)-1-(Azulen-1-yl)-2-(4-methylphenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 540-23-8
p-toluidine hydrochloride

: 275-51-4
azulene

: 93323-17-2
Azulene-1-azo-(4'-methylbenzene)

Guidance literature:: p-toluidine hydrochloride; With hydrogenchloride; sodium nitrite; at 0 ℃;

azulene; With sodium acetate; In ethanol; at 20 ℃; for 0.166667h;

Reference yield:

: 59775-82-5
5-[(4-methylphenyl)diazenyl]-4-phenyl-1,3-thiazol-2-amine

: 275-51-4
azulene

: 93323-17-2
Azulene-1-azo-(4'-methylbenzene)

: 2-[(azulen-1-yl)diazenyl]-4-phenyl-1,3-thiazole

: 2-(azulen-1-yldiazenyl)-4-phenyl-5-[(4-methylphenyl)diazenyl]-1,3-thiazole

Guidance literature:: 5-[(4-methylphenyl)diazenyl]-4-phenyl-1,3-thiazol-2-amine; With phosphoric acid; nitric acid; sodium nitrite; In water; at 0 ℃;

azulene; With potassium acetate; In methanol; water; at 0 ℃;
DOI:10.1002/jhet.5570400607

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 93323-17-2
Azulene-1-azo-(4'-methylbenzene)

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₃PO₄; HNO₃; NaNO₂ / H₂O / 0 °C

1.2: AcOK / methanol; H₂O / 0 °C

2.1: H₃PO₄; HNO₃; NaNO₂ / H₂O / 0 °C

2.2: AcOK / methanol; H₂O / 0 °C

With phosphoric acid; nitric acid; sodium nitrite; In water;
DOI:10.1002/jhet.5570400607