Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl-

Base Information

Chemical Name:Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl-
CAS No.:93667-57-3
Molecular Formula:C13H26N2O2
Molecular Weight:242.362
Hs Code.:
DSSTox Substance ID:DTXSID10366765
Wikidata:Q82152158

Synonyms:93667-57-3;Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl-;N,N'-(Propane-1,3-diyl)bis(2,2-dimethylpropanamide);N-[3-(2,2-Dimethylpropanamido)propyl]-2,2-dimethylpropanamide;N-[3-(2,2-dimethylpropanoylamino)propyl]-2,2-dimethylpropanamide;starbld0013111;SCHEMBL9355210;DTXSID10366765;STK439531;AKOS003326336;NCGC00332776-01;CS-0362411;AB00310112-03;SR-01000255080;N,N'-propane-1,3-diylbis(2,2-dimethylpropanamide);SR-01000255080-1

Suppliers and Price of Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl-

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:242.199428076
Heavy Atom Count:17
Complexity:244

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C(=O)NCCCNC(=O)C(C)(C)C

Technology Process of Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl-

There total 2 articles about Propanamide, N,N'-1,3-propanediylbis[2,2-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-76-2,54018-94-9
Trimethylenediamine

: 75-98-9
Trimethylacetic acid

: 754-10-9
2,2-dimethylpropionamide

: 14278-29-6
N-ethyl-2,2-dimethylpropanamide

: 93667-57-3
N,N'-(propane-1,3-diyl)bis(2,2-dimethylpropanamide)

: 92328-13-7
2-tert-butyl-1,4,5,6-tetrahydropyrimidine

Guidance literature:: aluminum oxide; palladium/alumina; for 91.3h; Further byproducts given. Title compound not separated from byproducts; 1) 275 deg C, 2) 320 deg C;
DOI:10.1021/jo00036a031

Reference yield:

: 109-76-2,54018-94-9
Trimethylenediamine

: 75-98-9
Trimethylacetic acid

: 754-10-9
2,2-dimethylpropionamide

: 14278-29-6
N-ethyl-2,2-dimethylpropanamide

: 93667-57-3
N,N'-(propane-1,3-diyl)bis(2,2-dimethylpropanamide)

: 92328-13-7
2-tert-butyl-1,4,5,6-tetrahydropyrimidine

: 61319-99-1
2-tert-butylpyrimidine

Guidance literature:: aluminum oxide; palladium/alumina; at 275 - 320 ℃; for 91.3h; Mechanism; Product distribution; other acid, other catalyst, other conditions;
DOI:10.1021/jo00036a031

Reference yield:

: 93667-57-3
N,N'-(propane-1,3-diyl)bis(2,2-dimethylpropanamide)

: N',N''-(propane-1,3-diyl)bis(N-(2,6-diisopropylphenyl)-2,2-dimethylpropanimidamide)

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentachloride / toluene / 72 h / 100 °C / Inert atmosphere; Schlenk technique

2: toluene / 48 h / Inert atmosphere; Schlenk technique; Reflux

With phosphorus pentachloride; In toluene;
DOI:10.1039/d0dt01923b