2-Cyclohexen-1-one, 4-(1,1-dimethylethyl)-

Base Information

• Chemical Name: 2-Cyclohexen-1-one, 4-(1,1-dimethylethyl)-
• CAS No.: 937-07-5
• Molecular Formula: C10H16O
• Molecular Weight: 152.236

Synonyms:4-(tert-butyl)-cyclohex-2-enone;4-tert-butylcyclohexen-1-one;4-tert-butylcyclohex-2-en-1-one;4-tert-butyl-2-cyclohexenone;4-tert-butyl-2-cyclohexen-1-one;

Chemical Property of 2-Cyclohexen-1-one, 4-(1,1-dimethylethyl)-

Chemical Property:

• PSA: 17.07000
• LogP: 2.56780

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-Cyclohexen-1-one, 4-(1,1-dimethylethyl)-

There total 21 articles about 2-Cyclohexen-1-one, 4-(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(phenylsulfinyl)-4-tert-butylcyclohexanone → 4-tert-butylcyclohex-2-enone (937-07-5)

Guidance literature:

With pyridinium p-toluenesulfonate; In tetrachloromethane; Heating;

DOI:10.1021/jo9807316

Reference yield: 95.0%

4-tercbutyl-cyclohexanone (98-53-3) → 4-tert-butylcyclohex-2-enone (937-07-5)

Guidance literature:

With iodic acid; dimethyl sulfoxide; at 50 ℃; for 8h;

DOI:10.1002/1521-3773(20020415)41:8<1386::AID-ANIE1386>3.0.CO;2-V

Reference yield: 91.0%

4-(1,1-dimethylethyl)-cyclohexanol (98-52-2) → 4-tert-butylcyclohex-2-enone (937-07-5)

Guidance literature:

With Oxone; sodium ortho-iodobenzenesulfonate; In nitromethane; at 70 ℃; for 5h;

upstream raw materials:

1-Methoxy-4-t-butyl-1,3-cyclohexadien

Cyclopentane

trans-4-tert-butyl-2-chloro-cyclohexanone

1-acetoxy-4-tert-butylcyclohexene

Downstream raw materials:

3-(1-Trimethylsilylvinyl)-4-t-butyl-cyclohexanon

(+)-(1R,4S)-4-t-Butyl-2-cyclohexen-1-ol

trans-4-tert-Butyl-2-cyclohexen-1-ol

4-tert-butyl-1-cyano-3-diethylphosphonooxy-1-cyclohexene

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