Benzene, 1-(methoxymethoxy)-2-(phenylmethoxy)-

Base Information

Chemical Name:Benzene, 1-(methoxymethoxy)-2-(phenylmethoxy)-
CAS No.:93758-13-5
Molecular Formula:C15H16O3
Molecular Weight:244.29
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-(methoxymethoxy)-2-(phenylmethoxy)-

Chemical Property:

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Technology Process of Benzene, 1-(methoxymethoxy)-2-(phenylmethoxy)-

There total 1 articles about Benzene, 1-(methoxymethoxy)-2-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6272-38-4
O-benzylcatechol

: 107-30-2
chloromethyl methyl ether

: 93758-13-5
2-<(methoxymethyl)oxy>-1-(benzyloxy)benzene

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, DMF, RT, 1.5 h, 2.) RT, 12 h;
DOI:10.1021/jo00202a014

Reference yield: 100.0%

: 93758-13-5
2-<(methoxymethyl)oxy>-1-(benzyloxy)benzene

: 6272-38-4
O-benzylcatechol

Guidance literature:: sodium hydrogen sulfate; silica gel; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo030088+

Reference yield:

: 93758-13-5
2-<(methoxymethyl)oxy>-1-(benzyloxy)benzene

: 93758-30-6
2,3,4,5,6,7,8,10-octahydro-2-benzyl-6,6-dimethoxyisoquinolino<5β,10β-c>-7-methoxy-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / H₂ / 5percent Pd/C / ethyl acetate; acetic acid / 4 h / 760 Torr

2: 59 percent / KH / tetrahydrofuran / 1.) RT, 3 h, 2.) reflux, 19 h

3: 1.) H₂O, AcOH, 2.) pyridine / 1.) THF, 80 deg C, 15 h, 2.) CH₂Cl₂, RT, 12 h

4: 99 percent / benzene; methanol; acetic acid / 6 h / Irradiation

5: 74 percent / concd. H₂SO₄ / methanol / 1.) reflux, 6 h, 2.) RT, 12 h

6: 72 percent / K₂CO₃ / acetone / 12 h / Heating

7: 90 percent / diisobutylaluminium hydride / tetrahydrofuran; hexane / 0.2 h / 0 °C

With pyridine; sulfuric acid; water; hydrogen; potassium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; acetic acid; ethyl acetate; acetone; benzene;
DOI:10.1021/jo00202a014