Methyl 2-(diethoxymethyl)-6-methoxybenzoate

Base Information

Chemical Name:Methyl 2-(diethoxymethyl)-6-methoxybenzoate
CAS No.:93832-27-0
Molecular Formula:C14H20O5
Molecular Weight:268.31
Hs Code.:
DSSTox Substance ID:DTXSID80534131
Wikidata:Q82407788

Synonyms:Methyl 2-(diethoxymethyl)-6-methoxybenzoate;93832-27-0;DTXSID80534131

Suppliers and Price of Methyl 2-(diethoxymethyl)-6-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-(diethoxymethyl)-6-methoxybenzoate

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:268.13107373
Heavy Atom Count:19
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(C1=C(C(=CC=C1)OC)C(=O)OC)OCC

Technology Process of Methyl 2-(diethoxymethyl)-6-methoxybenzoate

There total 1 articles about Methyl 2-(diethoxymethyl)-6-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2886-59-1
1-methoxycyclohexa-1,4-diene

: 93832-26-9
4,4-diethoxybut-2-ynoic acid methyl ester

: 93832-27-0
2-diethoxymethyl-6-methoxybenzoic acid methyl ester

Guidance literature:: In toluene; at 165 ℃; for 6h;
DOI:10.1021/jo00206a016

Reference yield:

: 93832-27-0
2-diethoxymethyl-6-methoxybenzoic acid methyl ester

: 2-(2-iodovinyl)-6-methoxybenzoic acid 4-methoxybenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / HCl; acetic acid / Heating

2: diisopropylethylamine / dimethylformamide / 100 °C

3: chromium(II) chloride / tetrahydrofuran / 5 h / 0 °C

With chromium dichloride; hydrogenchloride; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 3: Takai olefination;
DOI:10.1021/ol036007d

Reference yield:

: 93832-27-0
2-diethoxymethyl-6-methoxybenzoic acid methyl ester

: 651043-64-0
2-(2-iodovinyl)-6-methoxybenzoic acid 4-methoxybenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / HCl; acetic acid / Heating

2: diisopropylethylamine / dimethylformamide / 100 °C

3: 1.24 g / chromium(II) chloride / tetrahydrofuran / 5 h / 0 °C

With chromium dichloride; hydrogenchloride; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 3: Takai olefination;
DOI:10.1021/ol036007d