But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate

Base Information

Chemical Name:But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate
CAS No.:95602-06-5
Molecular Formula:C12H15NO4S
Molecular Weight:269.321
Hs Code.:
DSSTox Substance ID:DTXSID10537897
Nikkaji Number:J1.423.004A

Synonyms:95602-06-5;But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate;DTXSID10537897

Suppliers and Price of But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:269.07217913
Heavy Atom Count:18
Complexity:391

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC(=O)OC(C)C=C

Technology Process of But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate

There total 1 articles about But-3-en-2-yl (4-methylbenzene-1-sulfonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 598-32-3
2-hydroxy-3-butene

: 4083-64-1
Tosyl isocyanate

: 95602-06-5
O-but-3-en-2-yl N-tosylcarbamate

Guidance literature:: With triethylamine; In diethyl ether; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/anie.201100718

Reference yield: 87.0%

: 95602-06-5
O-but-3-en-2-yl N-tosylcarbamate

: C₁₂H₁₅NO₅S

Guidance literature:: With dihydrogen peroxide; palladium diacetate; lithium trifluoroacetate; In water; acetone; at -5 ℃; for 10h; diastereoselective reaction;
DOI:10.1021/ja412023b

Reference yield: 61.0%

: 95602-06-5
O-but-3-en-2-yl N-tosylcarbamate

: (4S*,5S*)-4-(azidomethyl)-5-methyl-3-tosyloxazolidin-2-one

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); sodium azide; dihydrogen peroxide; In tetrahydrofuran; water; at 25 ℃; for 24h;
DOI:10.1021/acs.orglett.0c00010