Benzenemethanamine,R-ethenyl-

Base Information

• Chemical Name: Benzenemethanamine,R-ethenyl-
• CAS No.: 4393-21-9
• Molecular Formula: C9H11N
• Molecular Weight: 133.193
• Hs Code.: 2921499090
• Mol file: 4393-21-9.mol

Synonyms:

Chemical Property of Benzenemethanamine,R-ethenyl-

Chemical Property:

• Boiling Point: 57 °C(Press: 0.07 Torr)
• PSA: 26.02000
• Density: 1.010 g/cm3(Temp: 25 °C)
• LogP: 2.57270

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine,R-ethenyl-

There total 21 articles about Benzenemethanamine,R-ethenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-<1-(1-phenylprop-2-enyl)> trichloroacetamide (59874-90-7) → 1-(phenyl)allylamine (4393-21-9)

Guidance literature:

With sodium hydroxide; In ethanol; for 48h;

Reference yield: 81.0%

Methyl N-(1-phenylprop-2-enyl)carbamate (86766-60-1) → 1-(phenyl)allylamine (4393-21-9)

Guidance literature:

With trimethylsilyl iodide; sodium iodide; In acetonitrile; for 24h; Heating;

DOI:10.1021/jo00168a040

Reference yield: 71.0%

N-(3-phenylpropen-3-yl)-4-nitrobenzenesulfonamide → 1-(phenyl)allylamine (4393-21-9)

Guidance literature:

With lithium acetate monohydrate; mercaptoacetic acid; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/d1cc02283k

upstream raw materials:

Vinyl-phenyl-acetamid

Methyl N-(1-phenylprop-2-enyl)carbamate

N-<1-(1-phenylprop-2-enyl)> trichloroacetamide

cinnamyl(phenyl)sulfide

Downstream raw materials:

3-phenyl-2-propenyl thiocyanate

(1-phenyl-allyl)-carbamic acid tert-butyl ester

(1-Phenyl-allyl)-(3-trifluoromethyl-benzyl)-amine

(2,4-Dimethyl-benzyl)-(1-phenyl-allyl)-amine