Silane, dimethyl[(2Z)-1-(1-methylethyl)-2-butenyl]phenyl-

Base Information

Chemical Name:Silane, dimethyl[(2Z)-1-(1-methylethyl)-2-butenyl]phenyl-
CAS No.:97946-14-0
Molecular Formula:C15H24Si
Molecular Weight:232.43700
Hs Code.:

Synonyms:(Z)-3-dimethyl(phenyl)silyl-2-methylhex-4-ene;((Z)-1-Isopropyl-but-2-enyl)-dimethyl-phenyl-silane;(Z)-4-dimethyl(phenyl)silyl-5-methylhex-2-ene;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, dimethyl[(2Z)-1-(1-methylethyl)-2-butenyl]phenyl-

Chemical Property:

PSA：0.00000
LogP:4.20430

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Silane, dimethyl[(2Z)-1-(1-methylethyl)-2-butenyl]phenyl-

There total 13 articles about Silane, dimethyl[(2Z)-1-(1-methylethyl)-2-butenyl]phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: (2RS,3SR)-2-<(SR)-1-dimethyl(phenyl)silyl-2-methylpropyl>-3-methylpropan-3-olide

: 97946-14-0
(+/-)-(Z)-3-(dimethylphenylsilyl)-2-methyl-4-hexene

Guidance literature:: With 2,4,6-trimethyl-pyridine; Heating; 4-5 h;

Reference yield:

: 106995-80-6
benzyl 3-dimethyl(phenyl)silyl-4-methylpentanoate

: 97946-14-0
(+/-)-(Z)-3-(dimethylphenylsilyl)-2-methyl-4-hexene

Guidance literature:: Multi-step reaction with 5 steps

1: i-Pr₂NLi / tetrahydrofuran / -78 °C

2: tetrahydrofuran / 1 h / -78 °C

3: H₂ / Pd

4: 61 percent / PhSO₂Cl / pyridine / 12 h / 0 °C

5: collidine / 5 h / Heating

With 2,3,5-trimethyl-pyridine; hydrogen; benzenesulfonyl chloride; lithium diisopropyl amide; palladium; In tetrahydrofuran; pyridine;
DOI:10.1039/c39860001199

Reference yield:

: 1068-55-9
isopropylmagnesium chloride

: 219666-72-5
(+/-)-1-(E)-(dimethylphenylsilyl)-1-buten-3-ol N-phenylcarbamate

: 97946-14-0
(+/-)-(Z)-3-(dimethylphenylsilyl)-2-methyl-4-hexene

: 97946-10-6
(+/-)-(E)-3-(dimethylphenylsilyl)-2-methyl-4-hexene

: ((E)-3,4-Dimethyl-pent-1-enyl)-dimethyl-phenyl-silane

Guidance literature:: With n-butyllithium; copper(I) iodide-lithium chloride; In tetrahydrofuran; hexane; at -78 - 22 ℃; for 16.5h;
DOI:10.1021/jo991312r