ethyl (E)-4-(dimethylamino)but-2-enoate

Base Information

Chemical Name:ethyl (E)-4-(dimethylamino)but-2-enoate
CAS No.:98552-51-3
Molecular Formula:C8H15NO2
Molecular Weight:157.213
Hs Code.:
European Community (EC) Number:619-363-7
UNII:Y4GT5VCZ6S

Synonyms:ethyl (E)-4-(dimethylamino)but-2-enoate;1086268-91-8;Ethyl 4-(dimethylamino)but-2-enoate;Y4GT5VCZ6S;(2E)-4-(Dimethylamino)-2-butenoic acid ethyl ester;Ethyl (2E)-4-(dimethylamino)-2-butenoate;UNII-Y4GT5VCZ6S;ethyl (2E)-4-(dimethylamino)but-2-enoate;4-(Dimethylamino)-2-butenoic acid ethyl ester, (2E)-;98552-51-3;2-Butenoic acid, 4-(dimethylamino)-, ethyl ester, (2E)-;SCHEMBL663907;SCHEMBL663908;MFCD22412766;AKOS019113638;BS-14355;CS-0162248;D80188;EN300-741845

Suppliers and Price of ethyl (E)-4-(dimethylamino)but-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of ethyl (E)-4-(dimethylamino)but-2-enoate

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:157.110278721
Heavy Atom Count:11
Complexity:141

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C=CCN(C)C
Isomeric SMILES:CCOC(=O)/C=C/CN(C)C

Technology Process of ethyl (E)-4-(dimethylamino)but-2-enoate

There total 2 articles about ethyl (E)-4-(dimethylamino)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 3616-56-6
dimethylaminoacetaldehyde diethyl acetal

: 98552-51-3,1086268-91-8
ethyl 4-(dimethylamino)crotonate

Guidance literature:: dimethylaminoacetaldehyde diethyl acetal; With hydrogenchloride; In water; at 0.2 - 0.7 ℃; for 0.12h;

With potassium hydroxide; In water; at 0 - 0.1 ℃; pH=9;

diethoxyphosphoryl-acetic acid ethyl ester; With potassium hydroxide; In 2-methyltetrahydrofuran; water; at 0 - 0.5 ℃; for 0.1h; pH=Ca.13.5;

Reference yield:

: 98552-51-3,1086268-91-8
ethyl 4-(dimethylamino)crotonate

Guidance literature:: 4-Dimethylamino-butin-(2)-saeure-aethylester, H2, Pd-Al2O3;

Reference yield: 63.0%

: 98552-51-3,1086268-91-8
ethyl 4-(dimethylamino)crotonate

: 98548-81-3,1130155-48-4
trans-4-dimethylaminocrotonic acid hydrochloride

Guidance literature:: ethyl 4-(dimethylamino)crotonate; With water; sodium hydroxide; In ethanol; at 0.25 - 0.55 ℃; for 0.1h;

With hydrogenchloride; In ethanol; at 5 ℃; pH=1.5;