Piperidine, 1-methyl-4-(1-phenylhydrazino)-

Base Information

Chemical Name:Piperidine, 1-methyl-4-(1-phenylhydrazino)-
CAS No.:99918-48-6
Molecular Formula:C12H19N3
Molecular Weight:205.29900
Hs Code.:

Synonyms:N-(1-Methyl-piperidin-4-yl)-N-phenyl-hydrazine;N-amino-N-(1-methyl-4-piperidinyl)aniline;N-(1-methyl-4-piperidinyl)-N-phenylhydrazine;

Suppliers and Price of Piperidine, 1-methyl-4-(1-phenylhydrazino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Piperidine, 1-methyl-4-(1-phenylhydrazino)-

Chemical Property:

Melting Point:58 - 60 °C
PSA：32.50000
LogP:2.09910

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Piperidine, 1-methyl-4-(1-phenylhydrazino)-

There total 4 articles about Piperidine, 1-methyl-4-(1-phenylhydrazino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 99918-47-5
N-(1-methyl-4-piperidinyl)-N-nitrosoaniline

: 99918-48-6
N-(1-methyl-piperidin-4-yl)-N-phenyl-hydrazine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h;

Reference yield:

: 22261-94-5
N-(1-methyl-4-piperidinyl)aniline

: 99918-48-6
N-(1-methyl-piperidin-4-yl)-N-phenyl-hydrazine

Guidance literature:: With hydrogenchloride; lithium aluminium tetrahydride; sodium nitrite; Yield given. Multistep reaction; 2) THF;
DOI:10.1016/0960-894X(95)00560-G

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 99918-48-6
N-(1-methyl-piperidin-4-yl)-N-phenyl-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) molecular sieves; 2) NaBH₄ / 1) benzene, reflux, 20 h; 2) EtOH, room temp., 5 h

2: 97 percent / conc. aq. HCl, aq. NaNO₂ / ethanol / 1 h / -10 °C

3: 77 percent / LiAlH₄ / diethyl ether / 3 h

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; molecular sieve; sodium nitrite; In diethyl ether; ethanol;