Technology Process of 6-Heptenoic acid, 7-[2-(heptyloxy)-3-(phenylmethoxy)cyclopentyl]-, [1R-[1a(Z),2b,3a]]-
There total 10 articles about 6-Heptenoic acid, 7-[2-(heptyloxy)-3-(phenylmethoxy)cyclopentyl]-, [1R-[1a(Z),2b,3a]]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 60 percent / NaH / dimethylformamide / 7 h / Ambient temperature
2: 83 percent / Raney nickel / acetone; ethanol / 16 h / Heating
3: 100 percent / 80 percent aq. formic acid / CHCl3 / Ambient temperature
4: 1.) sodium hydride / 1.) hexane, DMSO, 70 deg C, 1 h; 2.) r.t., 1 h, DMSO; 3.) r.t., 14 h
With
formic acid; sodium hydride;
nickel;
In
ethanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.19830660508
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 60 percent / NaH / dimethylformamide / 7 h / Ambient temperature
2: 83 percent / Raney nickel / acetone; ethanol / 16 h / Heating
3: 100 percent / 80 percent aq. formic acid / CHCl3 / Ambient temperature
4: 1.) sodium hydride / 1.) hexane, DMSO, 70 deg C, 1 h; 2.) r.t., 1 h, DMSO; 3.) r.t., 14 h
With
formic acid; sodium hydride;
nickel;
In
ethanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.19830660508
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 83 percent / Raney nickel / acetone; ethanol / 16 h / Heating
2: 100 percent / 80 percent aq. formic acid / CHCl3 / Ambient temperature
3: 1.) sodium hydride / 1.) hexane, DMSO, 70 deg C, 1 h; 2.) r.t., 1 h, DMSO; 3.) r.t., 14 h
With
formic acid; sodium hydride;
nickel;
In
ethanol; chloroform; acetone;
DOI:10.1002/hlca.19830660508
