(+/-)-1-(2,5-DIMETHOXY-4-IODOPHENYL)-2-AMINOPROPANE HYDROCHLORIDE

Base Information

Chemical Name:(+/-)-1-(2,5-DIMETHOXY-4-IODOPHENYL)-2-AMINOPROPANE HYDROCHLORIDE
CAS No.:82830-44-2
Molecular Formula:C₁₁H₁₆INO₂*ClH
Molecular Weight:357.619
Hs Code.:
Mol file:82830-44-2.mol

Synonyms:1-(2,5-Dimethoxy-4-iodophenyl)-2-aminopropane hydrochloride; 2,5-Dimet

Suppliers and Price of (+/-)-1-(2,5-DIMETHOXY-4-IODOPHENYL)-2-AMINOPROPANE HYDROCHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
DOI Hydrochloride
1mg
$ 340.00

Tocris
DOIhydrochloride ≥98%(HPLC)
10
$ 144.00

Total 27 raw suppliers

Chemical Property of (+/-)-1-(2,5-DIMETHOXY-4-IODOPHENYL)-2-AMINOPROPANE HYDROCHLORIDE

Chemical Property:

Melting Point:200-202 °C
PSA：44.48000
LogP:3.70040
Solubility.:H2O: 10 mg/mL

Purity/Quality:

97% ^*data from raw suppliers

DOI Hydrochloride ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 22-26-36

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+/-)-1-(2,5-DIMETHOXY-4-IODOPHENYL)-2-AMINOPROPANE HYDROCHLORIDE

There total 4 articles about (+/-)-1-(2,5-DIMETHOXY-4-IODOPHENYL)-2-AMINOPROPANE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 82830-50-0
(+/-)-N-acetyl-1-(2,5-dimethoxy-4-iodophenyl)-2-aminopropane

: 42203-78-1,82830-44-2
4-iodo-2,5-dimethoxyphenylisopropylamine hydrochloride

Guidance literature:: DOI:10.1021/jm00352a013

Reference yield:

: 42311-16-0
(+/-)-N-acetyl-1-(2,5-dimethoxyphenyl)-2-aminopropane

: 42203-78-1,82830-44-2
4-iodo-2,5-dimethoxyphenylisopropylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 2.21 g / silver trifluoroacetate, I₂ / CHCl₃ / 18 h

2: 71 percent

With iodine; silver trifluoroacetate; In chloroform;
DOI:10.1021/jm00352a013

Reference yield:

: N-[(R)-2-(2,5-Dimethoxy-phenyl)-1-methyl-ethyl]-acetamide

: 82830-44-2
(-)-DOI hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / silver trifluoroacetate, I₂ / CHCl₃ / 18 h

2: 1.) NaOH

With sodium hydroxide; iodine; silver trifluoroacetate; In chloroform;
DOI:10.1021/jm00352a013