TRIBUTYLMETHYLAMMONIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE

Base Information

• Chemical Name: TRIBUTYLMETHYLAMMONIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE
• CAS No.: 405514-94-5
• Molecular Formula: C₁₅H₃₀F₆N₂O₄S₂
• Molecular Weight: 480.5301
• Hs Code.: 29350090
• Mol file: 405514-94-5.mol

Synonyms:N,N-Dibut; Tributylmethylammonium Bis(trifluoromethanesulfonyl)imide

Chemical Property of TRIBUTYLMETHYLAMMONIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE

Chemical Property:

• Refractive Index: 1.4260-1.4300
• PSA: 85.04000
• Density: 1.27g/ml
• LogP: 7.05420
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

N,N-Dibutyl-N-methylbutan-1-aminiumbis((trifluoromethyl)sulfonyl)amide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TRIBUTYLMETHYLAMMONIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE

There total 2 articles about TRIBUTYLMETHYLAMMONIUM BIS(TRIFLUOROMETHYLSULFONYL)IMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl tributylammonium chloride + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → tributylmethylammonium bis(trifluoromethanesulfonyl)imide salt (405514-94-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 24h; Schlenk technique; Glovebox;

DOI:10.1002/anie.201507644

Reference yield:

tributyl-amine (102-82-9) + dimethyl sulfate (77-78-1) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → tributylmethylammonium bis(trifluoromethanesulfonyl)imide salt (405514-94-5)

Guidance literature:

tributyl-amine; dimethyl sulfate; In acetonitrile; at 0 - 20 ℃;

bis(trifluoromethane)sulfonimide lithium; In water;

DOI:10.1039/b901582e

Reference yield: 20.0%

benzyltrimethylazanium tetrachloro-λ3-iodanuide (121309-88-4) + tributylmethylammonium bis(trifluoromethanesulfonyl)imide salt (405514-94-5) → Cl4I(1-)*Cl3I2(1-)*2C10H16N(1+)

Guidance literature:

With bismuth(III) bromide; 18-crown-6 ether; at 50 ℃; for 24h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1016/j.molstruc.2018.03.125

upstream raw materials:

bis(trifluoromethane)sulfonimide lithium

tributyl-amine

dimethyl sulfate

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