3-Pyrrolidineacetic acid,hydrochloride

Base Information

• Chemical Name: 3-Pyrrolidineacetic acid,hydrochloride
• CAS No.: 80616-50-8
• Molecular Formula: C₆H₁₁NO₂*ClH
• Molecular Weight: 165.62
• Hs Code.: 2933990090
• Mol file: 80616-50-8.mol

Synonyms:(Pyrrolidin-3-yl)acetic acid hydrochloride;3-(Carboxymethyl)pyrrolidine hydrochloride, 3-(Carboxymethyl)tetrahydropyrrole hydrochloride

Chemical Property of 3-Pyrrolidineacetic acid,hydrochloride

Chemical Property:

• PSA: 49.33000
• LogP: 1.20140
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-PyrrolidineaceticAcidHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Pyrrolidineacetic acid,hydrochloride

There total 4 articles about 3-Pyrrolidineacetic acid,hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

methyl 1-methoxycarbonylpyrrolidine-3-acetate (80616-49-5) → homo-β-proline hydrochloride (80616-50-8)

Guidance literature:

With hydrogenchloride; for 1.5h; Heating;

Reference yield:

N-methoxycarbonyl-3-pyrrolidone (69079-09-0) → homo-β-proline hydrochloride (80616-50-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 62 percent / piperidine / pyridine / 12 h / Heating

2: 89 percent / H₂ / Pd-C / ethanol / 21 h / 2250.2 Torr

3: 50 percent / aq. HCl / Ambient temperature

4: 68 percent / aq. HCl / 1.5 h / Heating

With piperidine; hydrogenchloride; hydrogen; palladium on activated charcoal; In pyridine; ethanol;

Reference yield:

1-methoxycarbonyl-3-cyanomethyl-2-pyrroline (80616-47-3) → homo-β-proline hydrochloride (80616-50-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 89 percent / H₂ / Pd-C / ethanol / 21 h / 2250.2 Torr

2: 50 percent / aq. HCl / Ambient temperature

3: 68 percent / aq. HCl / 1.5 h / Heating

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;

upstream raw materials:

methyl 1-methoxycarbonylpyrrolidine-3-acetate

N-methoxycarbonyl-3-pyrrolidone

1-methoxycarbonyl-3-cyanomethyl-2-pyrroline

1-methoxycarbonyl-3-cyanomethyl-2-pyrrolidine

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