Benzoic acid,3-[(2-chloro-4-nitrophenoxy)methyl]-

Base Information

• Chemical Name: Benzoic acid,3-[(2-chloro-4-nitrophenoxy)methyl]-
• CAS No.: 30880-72-9
• Molecular Formula: C14H10 Cl N O5
• Molecular Weight: 307.69
• Mol file: 30880-72-9.mol

Synonyms:m-Toluicacid, a-(2-chloro-4-nitrophenoxy)-(8CI); NSC 146848; a-(2-Chloro-4-nitrophenoxy)-m-toluic acid

Chemical Property of Benzoic acid,3-[(2-chloro-4-nitrophenoxy)methyl]-

Chemical Property:

• Vapor Pressure: 1.32E-11mmHg at 25°C
• Boiling Point: 519.2°Cat760mmHg
• PKA: 4.09±0.10(Predicted)
• Flash Point: 267.8°C
• PSA: 92.35000
• Density: 1.461g/cm³
• LogP: 4.04860
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

3-((2-Chloro-4-nitrophenoxy)methyl)benzoicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid,3-[(2-chloro-4-nitrophenoxy)methyl]-

There total 3 articles about Benzoic acid,3-[(2-chloro-4-nitrophenoxy)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(2-Chloro-4-nitro-phenoxymethyl)-benzoic acid ethyl ester (30880-71-8) → 3-(2-chloro-4-nitro-phenoxymethyl)-benzoic acid (30880-72-9)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/jm00300a032

Reference yield:

ethyl 3-methylbenzoate (120-33-2) → 3-(2-chloro-4-nitro-phenoxymethyl)-benzoic acid (30880-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NBS, (PhCO)2O₂, (ii) /BRN= 2046372/, K₂CO₃

2: aq. NaOH

With sodium hydroxide;

DOI:10.1021/jm00300a032

Reference yield:

2-chloro-4-nitrophenol (619-08-9) → 3-(2-chloro-4-nitro-phenoxymethyl)-benzoic acid (30880-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NBS, (PhCO)2O₂, (ii) /BRN= 2046372/, K₂CO₃

2: aq. NaOH

With sodium hydroxide;

DOI:10.1021/jm00300a032

upstream raw materials:

3-(2-Chloro-4-nitro-phenoxymethyl)-benzoic acid ethyl ester

ethyl 3-methylbenzoate

2-chloro-4-nitrophenol

Downstream raw materials:

3-(2-Chloro-4-nitro-phenoxymethyl)-N,N-diethyl-benzamide

3-(2-Chloro-4-nitro-phenoxymethyl)-N-phenyl-benzamide

3-(2-Chloro-4-nitro-phenoxymethyl)-N-methyl-N-phenyl-benzamide

3-[(2-chloro-4-nitrophenoxy)methyl]-N,N-dimethylbenzamide