4-Chloro-n-[4-(dimethylamino)benzylidene]aniline

Base Information

• Chemical Name: 4-Chloro-n-[4-(dimethylamino)benzylidene]aniline
• CAS No.: 15486-62-1
• Molecular Formula: C15H15 Cl N2
• Molecular Weight: 258.75
• European Community (EC) Number: 653-527-9
• NSC Number: 158145
• Nikkaji Number: J387.775B
• Mol file: 15486-62-1.mol

Synonyms:4-chloro-n-[4-(dimethylamino)benzylidene]aniline;NSC158145;AKOS000343904;AKOS024333432;NSC-158145;15486-62-1

Chemical Property of 4-Chloro-n-[4-(dimethylamino)benzylidene]aniline

Chemical Property:

• Vapor Pressure: 1.19E-06mmHg at 25°C
• Boiling Point: 401.4°Cat760mmHg
• Flash Point: 196.5°C
• Density: 1.07g/cm³
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 258.0923762
• Heavy Atom Count: 18
• Complexity: 262

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)C=NC2=CC=C(C=C2)Cl

Technology Process of 4-Chloro-n-[4-(dimethylamino)benzylidene]aniline

There total 4 articles about 4-Chloro-n-[4-(dimethylamino)benzylidene]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-chloro-aniline (106-47-8) + 4-dimethylamino-benzaldehyde (100-10-7) → 4-chloro-N-(4-dimethylaminobenzylidene)aniline (15486-62-1)

Guidance literature:

In neat(no solvent); at 110 ℃; for 0.0166667h; Microwave irradiation;

DOI:10.1002/jhet.604

Reference yield: 80.0%

2-methoxy-5-<<(4-chlorophenyl)imino>methyl>phenol (115095-36-8) + 4-(N,N-dimethylamino)benzaldehyde 4-nitrophenylhydrazone (3155-30-4) → 4-chloro-N-(4-dimethylaminobenzylidene)aniline (15486-62-1)

Guidance literature:

With tetraethylammonium perchlorate; In acetonitrile; electrochemical oxidation;

DOI:10.1021/jo00256a033

Reference yield:

4-chloro-N-[(4-methoxyphenyl)methylidene]aniline (15485-22-0,98986-86-8,124397-44-0) + 4-(N,N-dimethylamino)benzaldehyde 4-nitrophenylhydrazone (3155-30-4) → 4-chloro-N-(4-dimethylaminobenzylidene)aniline (15486-62-1)

Guidance literature:

With tetraethylammonium perchlorate; In acetonitrile; electrochemical oxidation;

DOI:10.1021/jo00256a033

upstream raw materials:

4-chloro-aniline

4-dimethylamino-benzaldehyde

4-chloro-N-[(4-methoxyphenyl)methylidene]aniline

4-(N,N-dimethylamino)benzaldehyde 4-nitrophenylhydrazone

Downstream raw materials:

2,5-dibromo-3,6-bis-(4-chloro-anilino)-[1,4]benzoquinone

2,5-bis(4'-chloroanilino)-3,6-dichloro-1,4-benzoquinone

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