3-(1-oxa-4-azaspiro[4.5]dec-2-yl)phenol

Base Information

• Chemical Name: 3-(1-oxa-4-azaspiro[4.5]dec-2-yl)phenol
• CAS No.: 25283-29-8
• Molecular Formula: C14H19 N O2
• Molecular Weight: 233.3062
• Mol file: 25283-29-8.mol

Synonyms:Phenol,m-1-oxa-4-azaspiro[4.5]dec-2-yl- (8CI); 1-Oxa-4-azaspiro[4.5]decane, phenolderiv.

Chemical Property of 3-(1-oxa-4-azaspiro[4.5]dec-2-yl)phenol

Chemical Property:

• Vapor Pressure: 2.31E-07mmHg at 25°C
• Boiling Point: 411.6°Cat760mmHg
• Flash Point: 202.8°C
• PSA: 41.49000
• Density: 1.19g/cm³
• LogP: 3.04230

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(1-oxa-4-azaspiro[4.5]dec-2-yl)phenol

There total 3 articles about 3-(1-oxa-4-azaspiro[4.5]dec-2-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3'-hydroxyphenyl)-1-oxa-4-azospiro[4,5]decane hydrochloride + (+/-)-norphenylephrine hydrochloride (4779-94-6) → 5-(3-Hydroxyphenyl)-2-spirocyclohexanoxazolidine (25283-29-8)

Guidance literature:

In water; cyclohexanone; benzene;

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 1-(3-Trimethylsilyloxyphenyl)-1-trimethylsiloxy-2-trimethylsilalaminoethane (119610-78-5) → 5-(3-Hydroxyphenyl)-2-spirocyclohexanoxazolidine (25283-29-8)

Guidance literature:

In ethanol; Heating;

DOI:10.1007/BF00773617

Reference yield:

→ 5-(3-Hydroxyphenyl)-2-spirocyclohexanoxazolidine (25283-29-8)

Guidance literature:

1-<3-Hydroxy-phenyl>-2-amino-ethan-1-ol, Cyclohexanon, Ethanol, Siedetemp.;

upstream raw materials:

cyclohexanone

1-(3-Trimethylsilyloxyphenyl)-1-trimethylsiloxy-2-trimethylsilalaminoethane

(+/-)-norphenylephrine hydrochloride

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