(2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane

Base Information

Chemical Name:(2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane
CAS No.:60254-11-7
Molecular Formula:C19H17OPS
Molecular Weight:324.3764
Hs Code.:
NSC Number:346111
DSSTox Substance ID:DTXSID50319492
Nikkaji Number:J3.160.342K
Wikidata:Q82076007

Synonyms:60254-11-7;NSC 346111;2-diphenylthiophosphinylanisole;NSC346111;DTXSID50319492;(2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane;NSC-346111;Diphenyl(2-methoxyphenyl)phosphine sulfide

Suppliers and Price of (2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane

Chemical Property:

Vapor Pressure:1.8E-08mmHg at 25°C
Boiling Point:467.6°Cat760mmHg
Flash Point:236.6°C
Density:1.21g/cm³
XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:324.07377333
Heavy Atom Count:22
Complexity:363

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1P(=S)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of (2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane

There total 3 articles about (2-Methoxyphenyl)(diphenyl)sulfanylidene-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 529-28-2
4-iodoanisol

: 60254-11-7
(2-methoxyphenyl)diphenylphosphine sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; tris(trimethylsilyl)silane; 1,1'-azobis(cyclohexane-1-carbonitrile) / benzene / 20 h / Heating

2: 70 mg / sulfur / benzene / 1 h / 20 °C

With pyridine; tris-(trimethylsilyl)silane; sulfur; 1,1'-azobis(1-cyanocyclohexanenitrile); In benzene;
DOI:10.1021/ja058783h

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 60254-11-7
(2-methoxyphenyl)diphenylphosphine sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; tris(trimethylsilyl)silane; 1,1'-azobis(cyclohexane-1-carbonitrile) / benzene / 20 h / Heating

2: 70 mg / sulfur / benzene / 1 h / 20 °C

With pyridine; tris-(trimethylsilyl)silane; sulfur; 1,1'-azobis(1-cyanocyclohexanenitrile); In benzene;
DOI:10.1021/ja058783h