Benzyl benzyl(phenylsulfonyl)carbamate

Base Information

Chemical Name:Benzyl benzyl(phenylsulfonyl)carbamate
CAS No.:6629-36-3
Molecular Formula:C23H23NO5
Molecular Weight:381.4449
Hs Code.:
NSC Number:58147
UNII:QW4CHZ2U8M
DSSTox Substance ID:DTXSID70216499
Nikkaji Number:J839.087H
Wikidata:Q83092728

Synonyms:Benzyl benzyl(phenylsulfonyl)carbamate;6629-36-3;NSC 58147;NSC58147;NSC-58147;QW4CHZ2U8M;BENZYL N-(BENZENESULFONYL)-N-BENZYL-CARBAMATE;SCHEMBL6411443;DTXSID70216499;Benzyl benzyl(phenylsulphonyl)carbamate;Carbamic acid, (phenylmethyl)(phenylsulfonyl)-, phenylmethyl ester;Carbamic acid, (phenylmethyl)(phenylsulphonyl)-, phenylmethyl ester

Suppliers and Price of Benzyl benzyl(phenylsulfonyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Benzyl benzyl(phenylsulfonyl)carbamate

Chemical Property:

Vapor Pressure:6.53E-15mmHg at 25°C
Boiling Point:544.7°Cat760mmHg
Flash Point:283.2°C
Density:1.287g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:381.10347926
Heavy Atom Count:27
Complexity:553

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN(C(=O)OCC2=CC=CC=C2)S(=O)(=O)C3=CC=CC=C3

Technology Process of Benzyl benzyl(phenylsulfonyl)carbamate

There total 3 articles about Benzyl benzyl(phenylsulfonyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 837-18-3
N-benzylbenzenesulfonamide

: 501-53-1,94274-21-2
benzyl chloroformate

: 6629-36-3
N-benzyl-N-(benzyloxycarbonyl)benzenesulfonamide

Guidance literature:: With para-chlorotoluene; lithium; In tetrahydrofuran; at -40 - 20 ℃;

Reference yield:

: 175879-77-3
N-benzoyl-N-benzylbenzenesulfonamide

: 6629-36-3
N-benzyl-N-(benzyloxycarbonyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 74 percent / NaOMe / methanol / Heating

2.1: NaH / tetrahydrofuran / 1 h / 0 °C

2.2: tetrahydrofuran / 0 - 20 °C

With sodium methylate; sodium hydride; In tetrahydrofuran; methanol; 1.1: Deacylation / 2.1: Metallation / 2.2: Acylation;
DOI:10.1016/S0040-4020(00)00025-9