N-(3-oxo-3,4,4a,5,6,7-hexahydro-2H-benzo[6,7]cyclohepta[1,2-c]pyridazin-9-yl)acetamide

Base Information

Chemical Name:N-(3-oxo-3,4,4a,5,6,7-hexahydro-2H-benzo[6,7]cyclohepta[1,2-c]pyridazin-9-yl)acetamide
CAS No.:103602-79-5
Molecular Formula:C₁₅H₁₇N₃O₂
Molecular Weight:271.319
Hs Code.:

Synonyms:2H-Benzo[6,7]cyclohepta[1,2-c]pyridazine,acetamide deriv.

Suppliers and Price of N-(3-oxo-3,4,4a,5,6,7-hexahydro-2H-benzo[6,7]cyclohepta[1,2-c]pyridazin-9-yl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(3-oxo-3,4,4a,5,6,7-hexahydro-2H-benzo[6,7]cyclohepta[1,2-c]pyridazin-9-yl)acetamide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.38g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(3-oxo-3,4,4a,5,6,7-hexahydro-2H-benzo[6,7]cyclohepta[1,2-c]pyridazin-9-yl)acetamide

There total 3 articles about N-(3-oxo-3,4,4a,5,6,7-hexahydro-2H-benzo[6,7]cyclohepta[1,2-c]pyridazin-9-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 121866-01-1
(2-Acetylamino-5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-6-yl)-acetic acid

: 103602-79-5
9-(acetylamino)-2,4,4a,5,6,7-hexahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazin-3-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Heating;
DOI:10.1021/jm00130a009

Reference yield:

: 95207-74-2
2-(N-acetyl)amino-6,7,8,9-tetrahydrobenzo-cyclohepten-5-one

: 103602-79-5
9-(acetylamino)-2,4,4a,5,6,7-hexahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NaOH / H₂O / 3 h / Ambient temperature

2: 70 percent / Zn, AcOH / H₂O / Heating

3: 87 percent / H₂NNH₂*H₂O / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; acetic acid; zinc; In ethanol; water;
DOI:10.1021/jm00130a009

Reference yield:

: 103602-86-4
[2-Acetylamino-5-oxo-5,7,8,9-tetrahydro-benzocyclohepten-(6Z)-ylidene]-acetic acid

: 103602-79-5
9-(acetylamino)-2,4,4a,5,6,7-hexahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Zn, AcOH / H₂O / Heating

2: 87 percent / H₂NNH₂*H₂O / ethanol / 3 h / Heating

With hydrazine hydrate; acetic acid; zinc; In ethanol; water;
DOI:10.1021/jm00130a009