(2E)-2-hydroxyimino-6-methoxy-4,4-dimethyl-3H-naphthalen-1-one

Base Information

Chemical Name:(2E)-2-hydroxyimino-6-methoxy-4,4-dimethyl-3H-naphthalen-1-one
CAS No.:53503-63-2
Molecular Formula:C₁₃H₁₅NO₃
Molecular Weight:233.267
Hs Code.:
NSC Number:95167
DSSTox Substance ID:DTXSID70423464

Synonyms:NSC95167;53503-63-2;DTXSID70423464;NSC-95167

Suppliers and Price of (2E)-2-hydroxyimino-6-methoxy-4,4-dimethyl-3H-naphthalen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (2E)-2-hydroxyimino-6-methoxy-4,4-dimethyl-3H-naphthalen-1-one

Chemical Property:

Vapor Pressure:2.92E-07mmHg at 25°C
Boiling Point:404.3°C at 760 mmHg
Flash Point:198.3°C
Density:1.2g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:233.10519334
Heavy Atom Count:17
Complexity:349

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(=NO)C(=O)C2=C1C=C(C=C2)OC)C
Isomeric SMILES:CC1(C/C(=N\O)/C(=O)C2=C1C=C(C=C2)OC)C

Technology Process of (2E)-2-hydroxyimino-6-methoxy-4,4-dimethyl-3H-naphthalen-1-one

There total 1 articles about (2E)-2-hydroxyimino-6-methoxy-4,4-dimethyl-3H-naphthalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23203-51-2
6-methoxy-4,4-dimethyl-3,4-dihydronaphthalen-1(2H)-one

: 53503-63-2
3,4-dihydro-6-methoxy-4,4-dimethyl-1,2-naphthalenedione, 2-oxime

Guidance literature:: With sodium methylate; isopentyl nitrite; In methanol;
DOI:10.1248/cpb.23.1917

Reference yield:

: 53503-63-2
3,4-dihydro-6-methoxy-4,4-dimethyl-1,2-naphthalenedione, 2-oxime

: 2-(3-Amino-1.1-dimethylpropyl)-4-methoxy-benzoesaeure

Guidance literature:: Multi-step reaction with 2 steps

1: TsCl, aq. NaOH / benzene

2: H₂, aq. HCl / PtO₂ / ethanol

With hydrogenchloride; sodium hydroxide; hydrogen; p-toluenesulfonyl chloride; platinum(IV) oxide; In ethanol; benzene;
DOI:10.1248/cpb.23.1917

Reference yield:

: 53503-63-2
3,4-dihydro-6-methoxy-4,4-dimethyl-1,2-naphthalenedione, 2-oxime

: 53401-23-3
2-(3-Amino-1,1-dimethyl-propyl)-4-methoxy-benzylalkohol

Guidance literature:: Multi-step reaction with 3 steps

1: TsCl, aq. NaOH / benzene

2: HCl

3: LiAlH₄ / diethyl ether

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; p-toluenesulfonyl chloride; In diethyl ether; benzene;
DOI:10.1248/cpb.23.1917