(4aS,4bR,6aS,8S,10aS,10bS,12aS)-10a,12a-dimethyl-2-oxooctadecahydronaphtho[2,1-f]quinolin-8-yl 3-[bis(2-chloroethyl)amino]benzoate

Base Information

Chemical Name:(4aS,4bR,6aS,8S,10aS,10bS,12aS)-10a,12a-dimethyl-2-oxooctadecahydronaphtho[2,1-f]quinolin-8-yl 3-[bis(2-chloroethyl)amino]benzoate
CAS No.:157757-67-0
Molecular Formula:C₃₀H₄₂Cl₂N₂O₃
Molecular Weight:549.581
Hs Code.:

(4aS,4bR,6aS,8S,10aS,10bS,12aS)-10a,12a-dimethyl-2-oxooctadecahydronaphtho[2,1-f]quinolin-8-yl 3-[bis(2-chloroethyl)amino]benzoate

Synonyms:17a-Aza-D-homoandrostan-17-one,3-[[3-[bis(2-chloroethyl)amino]benzoyl]oxy]-, (3b,5a)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4aS,4bR,6aS,8S,10aS,10bS,12aS)-10a,12a-dimethyl-2-oxooctadecahydronaphtho[2,1-f]quinolin-8-yl 3-[bis(2-chloroethyl)amino]benzoate

Chemical Property:

Vapor Pressure:6.4E-19mmHg at 25°C
Boiling Point:690.6°C at 760 mmHg
Flash Point:371.4°C
Density:1.23g/cm³

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (4aS,4bR,6aS,8S,10aS,10bS,12aS)-10a,12a-dimethyl-2-oxooctadecahydronaphtho[2,1-f]quinolin-8-yl 3-[bis(2-chloroethyl)amino]benzoate

There total 6 articles about (4aS,4bR,6aS,8S,10aS,10bS,12aS)-10a,12a-dimethyl-2-oxooctadecahydronaphtho[2,1-f]quinolin-8-yl 3-[bis(2-chloroethyl)amino]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 39932-99-5
3β-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam

: 1026640-26-5
C₂₂H₂₄Cl₄N₂O₃

: 157757-67-0
3β-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam m-N,N-bis(2-chloroethyl)aminobenzoate

Guidance literature:: With dmap; In benzene; for 48h;
DOI:10.1002/jhet.5570310219

Reference yield: 72.0%

: 1704-46-7
3α-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam

: 1026640-26-5
C₂₂H₂₄Cl₄N₂O₃

: 157757-67-0
3α-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam m-N,N-bis(2-chloroethyl)aminobenzoate

Guidance literature:: With dmap; In benzene; for 48h;
DOI:10.1002/jhet.5570310219

Reference yield:

: 24813-11-4
3-N,N-bis(2-chloroethyl)aminobenzoyl chloride

: 157757-67-0
3α-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam m-N,N-bis(2-chloroethyl)aminobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / benzene / 2 h / Heating

2: 72 percent / 4-dimethylaminopyridine / benzene / 48 h

With pyridine; dmap; In benzene;
DOI:10.1002/jhet.5570310219