7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline

Base Information

Chemical Name:7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline
CAS No.:82589-56-8
Molecular Formula:C₁₆H₁₇N
Molecular Weight:223.318
Hs Code.:
DSSTox Substance ID:DTXSID101002806

Synonyms:BRN 4452666;7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline;Benzo(f)pyrrolo(1,2-b)isoquinoline, 7,9,10,11,11a,12-hexahydro-;82589-56-8;7,9,10,11,11a,12-Hexahydrobenzo[f]pyrrolo[1,2-b]isoquinoline;DTXSID101002806;LS-40153

Suppliers and Price of 7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline

Chemical Property:

Vapor Pressure:9.35E-06mmHg at 25°C
Boiling Point:372.8°Cat760mmHg
Flash Point:161.3°C
Density:1.16g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:223.136099547
Heavy Atom Count:17
Complexity:287

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2CC3=C(CN2C1)C=CC4=CC=CC=C34

Technology Process of 7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline

There total 7 articles about 7,9,10,11,11a,12-Hexahydrobenzo(f)pyrrolo(1,2-b)isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10,11,11a,12-Tetrahydro-9H-benzo[f]pyrrolo[1,2-b]isoquinolinylium; chloride

: 82589-56-8
7,9,10,11,11a,12-Hexahydrobenzopyrrolo<1,2-b>isoquinoline

Guidance literature:: With sodium tetrahydroborate; In methanol; Yield given; Ambient temperature;

Reference yield:

: 82589-42-2
2-[1]naphthylmethyl-pyrrolidine

: 82589-56-8
7,9,10,11,11a,12-Hexahydrobenzopyrrolo<1,2-b>isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 69.5 percent / Heating

2: POCl₃ / toluene / 95 °C

3: NaBH₄ / methanol / Ambient temperature

With sodium tetrahydroborate; trichlorophosphate; In methanol; toluene;

Reference yield:

: 66-77-3
1-naphthaldehyde

: 82589-56-8
7,9,10,11,11a,12-Hexahydrobenzopyrrolo<1,2-b>isoquinoline

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / piperidine acetate / toluene / Heating

2: 92 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 50percent aq. sulphuric acid / a. water removed, b. 130-140 deg C (15mm), 2h

4: 10percent aq. NaOH / Heating

5: 69.5 percent / Heating

6: POCl₃ / toluene / 95 °C

7: NaBH₄ / methanol / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; piperdinium acetate; trichlorophosphate; In tetrahydrofuran; methanol; toluene;