Toluene-2,4-disulfonamide

Base Information

Chemical Name:Toluene-2,4-disulfonamide
CAS No.:717-44-2
Molecular Formula:C7H10N2O4S2
Molecular Weight:250.299
Hs Code.:
NSC Number:49754
UNII:5674UBC61A
DSSTox Substance ID:DTXSID30287226
Wikidata:Q27261383

Synonyms:Toluene-2,4-disulfonamide;4-methylbenzene-1,3-disulfonamide;4-Methyl-1,3-benzenedisulfonamide;717-44-2;NSC-49754;1,3-Benzenedisulfonamide, 4-methyl-;UNII-5674UBC61A;5674UBC61A;NSC49754;Toluol-2,4-disulfamid;SCHEMBL1925948;DTXSID30287226;ZINC01681595;AKOS009345535;EN300-271786;Q27261383

Suppliers and Price of Toluene-2,4-disulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Toluene-2,4-disulfonamide

Chemical Property:

Vapor Pressure:3.18E-11mmHg at 25°C
Boiling Point:527.7°Cat760mmHg
Flash Point:273°C
Density:1.529g/cm³
XLogP3:-0.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:250.00819915
Heavy Atom Count:15
Complexity:417

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)S(=O)(=O)N)S(=O)(=O)N

Technology Process of Toluene-2,4-disulfonamide

There total 5 articles about Toluene-2,4-disulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2767-77-3
toluene-2,4-disulfonyl dichloride

: 717-44-2
4-methylbenzo-1,3-disulfonamide

Guidance literature:: With ammonium hydroxide; In water; at 100 ℃; for 2h;
DOI:10.1007/s10593-012-0948-8

Reference yield: 58.0%

: 104-15-4
toluene-4-sulfonic acid

: 717-44-2
4-methylbenzo-1,3-disulfonamide

Guidance literature:: toluene-4-sulfonic acid; With chlorosulfonic acid; at 150 ℃; for 6h;

With ammonium hydroxide; In water; at 0 ℃; for 3h;
DOI:10.1016/j.bmc.2011.09.003

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 717-44-2
4-methylbenzo-1,3-disulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 0.5 h / 145 °C

2: ammonium hydroxide / water / 2 h / Reflux

With chlorosulfonic acid; ammonium hydroxide; In water;
DOI:10.2174/1570180811310050007