2,4-Dichloro-3-phenylcyclobut-2-en-1-one

Base Information

Chemical Name:2,4-Dichloro-3-phenylcyclobut-2-en-1-one
CAS No.:16547-34-5
Molecular Formula:C10H6 Cl2 O
Molecular Weight:213.063
Hs Code.:
NSC Number:33252
DSSTox Substance ID:DTXSID40283754
Nikkaji Number:J619.815E
Mol file:16547-34-5.mol

Synonyms:16547-34-5;2,4-dichloro-3-phenylcyclobut-2-en-1-one;NSC33252;DTXSID40283754;NSC-33252

Suppliers and Price of 2,4-Dichloro-3-phenylcyclobut-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,4-Dichloro-3-phenylcyclobut-2-en-1-one

Chemical Property:

Vapor Pressure:0.00254mmHg at 25°C
Boiling Point:287.1°Cat760mmHg
Flash Point:119.8°C
Density:1.41g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:211.9795702
Heavy Atom Count:13
Complexity:264

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C(=O)C2Cl)Cl

Technology Process of 2,4-Dichloro-3-phenylcyclobut-2-en-1-one

There total 11 articles about 2,4-Dichloro-3-phenylcyclobut-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 3470-35-7
4,4-dichloro-3-phenyl-2-cyclobuten-1-one

: 16547-34-5
2,4-dichloro-3-phenyl-2-cyclobuten-1-one

Guidance literature:: With triphenylphosphonio-1-methylethanide; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4020(99)00695-X

Reference yield:

: 3470-35-7
4,4-dichloro-3-phenyl-2-cyclobuten-1-one

: 16547-34-5
2,4-dichloro-3-phenyl-2-cyclobuten-1-one

: 102170-63-8
2-Chloro-4-bromo-3-phenyl-2-cyclobutenone

Guidance literature:: With lithium bromide; In N,N-dimethyl-formamide; at 50 ℃; for 16h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00101a062

Reference yield:

: 3470-35-7
4,4-dichloro-3-phenyl-2-cyclobuten-1-one

: 16547-34-5
2,4-dichloro-3-phenyl-2-cyclobuten-1-one

: 98949-07-6
2-Chloro-4-iodo-3-phenyl-2-cyclobutenone

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 50 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00101a062