adamantyl nitroxide

Base Information

• Chemical Name: adamantyl nitroxide
• CAS No.: 55204-70-1
• Molecular Formula: C₁₄H₂₂NO₂
• Molecular Weight: 236.334
• Mol file: 55204-70-1.mol

Synonyms:adamantyl nitroxide

Chemical Property of adamantyl nitroxide

Chemical Property:

• PSA: 12.47000
• LogP: 2.53300

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of adamantyl nitroxide

There total 3 articles about adamantyl nitroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4',4'-dimethyl-spiro[adamantane-2,2'-oxazolidine] → Spiro(2,2'-adamantan<4',4'-dimethyloxazolidin-3-oxy>) (55204-70-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; at 20 ℃; for 2h;

DOI:10.1016/S0040-4039(01)86649-1

Reference yield:

2-Adamantanone (700-58-3) → Spiro(2,2'-adamantan<4',4'-dimethyloxazolidin-3-oxy>) (55204-70-1)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 65 h / 70 °C

2: MCPBA / diethyl ether / 2 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; benzene;

DOI:10.1016/S0040-4039(01)86649-1

Reference yield:

→ Spiro(2,2'-adamantan<4',4'-dimethyloxazolidin-3-oxy>) (55204-70-1)

Guidance literature:

Monooxazolidin,m-Chlorperbenzoesaeure;

DOI:10.1016/S0040-4039(01)86649-1

upstream raw materials:

2-Adamantanone