methyl 21-hydroxyibogamine-18-carboxylate

Base Information

• Chemical Name: methyl 21-hydroxyibogamine-18-carboxylate
• CAS No.: 77431-58-4
• Molecular Formula: C₂₁H₂₆N₂O₃
• Molecular Weight: 354.449

Synonyms:

Chemical Property of methyl 21-hydroxyibogamine-18-carboxylate

Chemical Property:

• Vapor Pressure: 2.5E-12mmHg at 25°C
• Boiling Point: 536.2°C at 760 mmHg
• PKA: 15.07±0.10(Predicted)
• Flash Point: 278.1°C
• PSA: 65.56000
• Density: 1.32g/cm³
• LogP: 2.16550

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 21-hydroxyibogamine-18-carboxylate

There total 4 articles about methyl 21-hydroxyibogamine-18-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

18-benzyloxycoronaridine → (+/-)-Albifloranine (77431-58-4)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol; for 4h; Heating;

DOI:10.1016/S0040-4020(99)00513-X

Reference yield:

C28H32N2O3 → (+/-)-Albifloranine (77431-58-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / toluene / 3 h / 130 °C

2: 75 percent / ammonium formate / Pd/C / methanol / 4 h / Heating

With ammonium formate; palladium on activated charcoal; In methanol; toluene; 1: Rearrangement / 2: Hydrogenolysis;

DOI:10.1016/S0040-4020(99)00513-X

Reference yield:

(9R,11R)-9-(4-Benzyloxy-2-[1,3]dioxolan-2-yl-butyl)-5,6,7,8,9,10,11,12-octahydro-7,12-diaza-cyclonona[a]indene-11-carboxylic acid methyl ester → (+/-)-Albifloranine (77431-58-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / HCl / H₂O; acetic acid; methanol / 24 h / 20 °C

2: 70 percent / toluene / 3 h / 130 °C

3: 75 percent / ammonium formate / Pd/C / methanol / 4 h / Heating

With hydrogenchloride; ammonium formate; palladium on activated charcoal; In methanol; water; acetic acid; toluene; 1: Hydrolysis / 2: Rearrangement / 3: Hydrogenolysis;

DOI:10.1016/S0040-4020(99)00513-X

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