2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride

Base Information

Chemical Name:2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride
CAS No.:100311-00-0
Molecular Formula:C₁₃H₁₈ClN*ClH
Molecular Weight:260.207
Hs Code.:
NSC Number:136005
DSSTox Substance ID:DTXSID20143145

Synonyms:100311-00-0;2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride;2-(2-Chloroethyl)-1,2,3,4,5,6-hexahydro-2-benzazocine hydrochloride;METHYLDOCOSAHEXAENOATE;DTXSID20143145;NSC136005;NSC-136005;LS-28039

Suppliers and Price of 2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride

Chemical Property:

Vapor Pressure:0.000288mmHg at 25°C
Boiling Point:322°Cat760mmHg
Flash Point:148.5°C
Density:g/cm³
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:259.0894550
Heavy Atom Count:16
Complexity:183

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCN(CC2=CC=CC=C2C1)CCCl.Cl

Technology Process of 2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride

There total 4 articles about 2-Benzazocine, 1,2,3,4,5,6-hexahydro-2-(2-chloroethyl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109187-61-3
2-(3,4,5,6-tetrahydro-1H-benz[c]azocin-2-yl)-ethanol

: 100311-00-0
2-(2-chloro-ethyl)-1,2,3,4,5,6-hexahydro-benz[c]azocine; hydrochloride

Guidance literature:: With thionyl chloride; chloroform;

Reference yield:

: 97729-16-3
2-(3-Methoxycarbonyl-propyl)-benzoic acid methyl ester

: 100311-00-0
2-(2-chloro-ethyl)-1,2,3,4,5,6-hexahydro-benz[c]azocine; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄; diethyl ether

2: chloroform; pyridine; thionyl chloride

3: ethanol / Erhitzen einer Loesung des Reaktionsprodukts in Propan-1,2-diol mit Kaliumcarbonat

4: chloroform; thionyl chloride

With pyridine; lithium aluminium tetrahydride; thionyl chloride; diethyl ether; ethanol; chloroform;

Reference yield:

: 934417-52-4
2-(4-hydroxybutyl)benzyl alcohol

: 100311-00-0
2-(2-chloro-ethyl)-1,2,3,4,5,6-hexahydro-benz[c]azocine; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform; pyridine; thionyl chloride

2: ethanol / Erhitzen einer Loesung des Reaktionsprodukts in Propan-1,2-diol mit Kaliumcarbonat

3: chloroform; thionyl chloride

With pyridine; thionyl chloride; ethanol; chloroform;