7,8-dimethoxy-1H-3-benzazepin-2-amine HCl

Base Information

• Chemical Name: 7,8-dimethoxy-1H-3-benzazepin-2-amine HCl
• CAS No.: 93270-40-7
• Molecular Formula: C₁₂H₁₄N₂O₂*ClH
• Molecular Weight: 254.716
• Hs Code.: 2933990090
• Mol file: 93270-40-7.mol

Synonyms:1H-3-Benzazepin-2-amine,7,8-dimethoxy-, monohydrochloride (9CI); LY 127210

Chemical Property of 7,8-dimethoxy-1H-3-benzazepin-2-amine HCl

Chemical Property:

• Vapor Pressure: 1.66E-06mmHg at 25°C
• Boiling Point: 396.9°Cat760mmHg
• Flash Point: 193.8°C
• PSA: 54.34000
• Density: g/cm³
• LogP: 3.02800

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7,8-dimethoxy-1H-3-benzazepin-2-amine HCl

There total 1 articles about 7,8-dimethoxy-1H-3-benzazepin-2-amine HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2,2-Dimethoxy-ethyl)-2-(3,4-dimethoxy-phenyl)-acetamidine; hydrochloride (93270-39-4) → 1-amino-2-(3,4-dimethoxyphenyl)ethan-1-imine hydrochloride (6487-89-4) + 8,9-Dimethoxy-11H-imidazo<2,1-b><3>benzazepine (125532-75-4) + 2-Amino-7,8-dimethoxy-1H-3-benzazepine Hydrochloride (93270-40-7) + 2,11-Dihydro-8,9-dimethoxy-3H-imidazo<2,1-b><3>benzazepin-3-ol Hydrochloride (125532-74-3)

Guidance literature:

With hydrogenchloride; In acetic acid; at 50 ℃; for 4h; Yield given. Further byproducts given;

DOI:10.1002/jhet.5570260350

upstream raw materials:

N-(2,2-Dimethoxy-ethyl)-2-(3,4-dimethoxy-phenyl)-acetamidine; hydrochloride