3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide

Base Information

Chemical Name:3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide
CAS No.:67755-09-3
Molecular Formula:C12H11NO2S
Molecular Weight:233.2862
Hs Code.:
DSSTox Substance ID:DTXSID60987085

Synonyms:3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide;67755-09-3;2H,6H-(1,3)Thiazolo(3,2-b)isoquinolin-6-one, 3,4-dihydro-, 1-oxide;6-Oxo-3,4-dihydro-2H,6H-1,3-thiazino(3,2-b)isoquinoline-1-oxide;SCHEMBL11233942;DTXSID60987085;LS-152015;3,4-Dihydro-2H-1lambda~4~-[1,3]thiazino[3,2-b]isoquinoline-1,6-dione

Suppliers and Price of 3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide

Chemical Property:

Vapor Pressure:5.28E-12mmHg at 25°C
Boiling Point:546.6°Cat760mmHg
Flash Point:284.4°C
Density:1.47g/cm³
XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:233.05104977
Heavy Atom Count:16
Complexity:377

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN2C(=CC3=CC=CC=C3C2=O)S(=O)C1

Technology Process of 3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide

There total 4 articles about 3,4-Dihydro-2H,6H-(1,3)thiazolo(3,2-b)isoquinolin-6-one 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67755-06-0
3,4-dihydro-2H-[1,3]thiazino[3,2-b]isoquinolin-6-one

: 67755-09-3
1-oxo-1,2,3,4-tetrahydro-1λ⁴-[1,3]thiazino[3,2-b]isoquinolin-6-one

Guidance literature:: With dihydrogen peroxide; In acetic acid; Ambient temperature;
DOI:10.1248/cpb.27.2372

Reference yield:

: 67755-50-4
2-(3-mercapto-propyl)-4H-isoquinoline-1,3-dione

: 67755-09-3
1-oxo-1,2,3,4-tetrahydro-1λ⁴-[1,3]thiazino[3,2-b]isoquinolin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH / 1,2-dichloro-benzene / 0.5 h / 120 °C

2: aq. H₂O₂ / acetic acid / Ambient temperature

With dihydrogen peroxide; toluene-4-sulfonic acid; In acetic acid; 1,2-dichloro-benzene;
DOI:10.1248/cpb.27.2372

Reference yield:

: 89-51-0
Homophthalic acid

: 67755-09-3
1-oxo-1,2,3,4-tetrahydro-1λ⁴-[1,3]thiazino[3,2-b]isoquinolin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: (i) NaOAc, 1,2-dichloro-benzene, (ii) TsOH

2: aq. H₂O₂ / acetic acid / Ambient temperature

With dihydrogen peroxide; In acetic acid;
DOI:10.1248/cpb.27.2372