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17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one

Base Information Edit
  • Chemical Name:17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one
  • CAS No.:116256-39-4
  • Molecular Formula:C21H28 O3
  • Molecular Weight:328.452
  • Hs Code.:
  • Mol file:116256-39-4.mol
17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one

Synonyms:17-ethynyl-9,17-dihydroxyandrost-4-en-3-one;EtdiOHandrostene-3-one

Suppliers and Price of 17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 1 raw suppliers
Chemical Property of 17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one Edit
Chemical Property:
  • Boiling Point:482.7°Cat760mmHg 
  • Flash Point:259.8°C 
  • PSA:57.53000 
  • Density:1.21g/cm3 
  • LogP:2.99750 
  • XLogP3:1.8
  • Hydrogen Bond Donor Count:2
  • Hydrogen Bond Acceptor Count:3
  • Rotatable Bond Count:1
  • Exact Mass:328.20384475
  • Heavy Atom Count:24
  • Complexity:684
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:CC12CCC3(C(C1CCC2(C#C)O)CCC4=CC(=O)CCC43C)O
  • Isomeric SMILES:C[C@]12CC[C@]3([C@H]([C@@H]1CC[C@]2(C#C)O)CCC4=CC(=O)CC[C@@]43C)O
Technology Process of 17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one

There total 5 articles about 17-Ethynyl-9,17-dihydroxyandrost-4-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 1.3 g / 5percent H2SO4 / methanol / 1 h / Ambient temperature
2: 0.708 g / ethylenediamine / tetrahydrofuran / 20 h / Ambient temperature
With sulfuric acid; ethylenediamine; In tetrahydrofuran; methanol;
DOI:10.1016/0039-128X(88)90002-5
Guidance literature:
Multi-step reaction with 3 steps
1: 4.0 g / ethane-1,2-diamine; tetrahydrofuran / 2.5 h / Ambient temperature
2: 1) LiBr, 15percent BuLi / 1) THF, hexane, -60 deg C, 45 min, 2) THF, hexane, -60 deg C, 45 min
3: 1) AgNO3, 2) 4 M aq. HCl / 1) THF, H2O, 2 h, 2) MeOH, H2O, r.t., 15 min
With hydrogenchloride; n-butyllithium; silver nitrate; lithium bromide; In tetrahydrofuran; ethylenediamine;
DOI:10.1016/0039-128X(89)90006-8
Guidance literature:
With ethylenediamine; In tetrahydrofuran; for 20h; Ambient temperature;
DOI:10.1016/0039-128X(88)90002-5
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