9-Anthryldiazomethane

Base Information

Chemical Name:9-Anthryldiazomethane
CAS No.:10401-59-9
Molecular Formula:C15H10N2
Molecular Weight:218.25
Hs Code.:2927000090
European Community (EC) Number:634-628-7
DSSTox Substance ID:DTXSID40146219
Nikkaji Number:J397.305K
Mol file:10401-59-9.mol

Synonyms:9-anthryldiazomethane;9-diazomethylanthracene

Suppliers and Price of 9-Anthryldiazomethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
9-Anthryldiazomethane
25mg
$ 270.00

Cayman Chemical
9-Anthryldiazomethane
25mg
$ 300.00

Cayman Chemical
9-Anthryldiazomethane
10mg
$ 135.00

Cayman Chemical
9-Anthryldiazomethane
5mg
$ 75.00

American Custom Chemicals Corporation
9-ANTHRYLDIAZOMETHANE 95.00%
25MG
$ 988.68

AK Scientific
9-Anthryldiazomethane
25mg
$ 505.00

Total 15 raw suppliers

Chemical Property of 9-Anthryldiazomethane

Chemical Property:

Melting Point:65-67 °C
PSA：37.39000
LogP:3.72276
Storage Temp.:−20°C
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:218.084398327
Heavy Atom Count:17
Complexity:297

Purity/Quality:

98%,99%, ^*data from raw suppliers

9-Anthryldiazomethane ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=C3C=CC=CC3=C2C=[N+]=[N-]
Uses Fluorescent probe for direct carboxylic acid modification. 9-Anthryldiazomethane (ADAM) is a fluorescent diazomethane analog used to identify bile acids, amino acids, fatty acids, steroid acids, and prostaglandins. In addition, derivatives of 9-Anthryldiazomethane can be detected using liquid chromatography-mass spectrometry. Furthermore, the fluorescence of these analogs can be detected at 254nm and 412 nm. Alternate studies indicate that 9-Anthryldiazomethane can be used to identify prostaglandins in plasma assays using HPLC.

Technology Process of 9-Anthryldiazomethane

There total 2 articles about 9-Anthryldiazomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 7512-18-7
anthracen-9-ylmethylene-hydrazone

: 10401-59-9
9-anthryldiazomethane

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1021/jo971589w

Reference yield:

: (E)‐(anthracen‐9‐ylmethylene)hydrazine

: 10401-59-9
9-anthryldiazomethane

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1021/ol070515w

Reference yield: 38.0%

: 14174-09-5
dibenzo-24-crown ether

: 10401-59-9
9-anthryldiazomethane

: C₁₉H₂₃NO₂*F₆P^(1-)*H⁽¹⁺⁾

: C₃₄H₃₃NO₂*C₂₄H₃₂O₈*F₆P^(1-)*H⁽¹⁺⁾

Guidance literature:: dibenzo-24-crown ether; C₁₉H₂₃NO₂*F₆P^(1-)*H⁽¹⁺⁾; In chloroform; acetonitrile;

9-anthryldiazomethane; In chloroform; acetonitrile; at 4 ℃; for 48h;
DOI:10.1246/cl.2002.810