N-Desmethyleclanamine

Base Information

Chemical Name:N-Desmethyleclanamine
CAS No.:116271-40-0
Molecular Formula:C₁₅H₂₀Cl₂N₂O
Molecular Weight:315.243
Hs Code.:
DSSTox Substance ID:DTXSID40151328
Wikidata:Q83017772
Mol file:116271-40-0.mol

Synonyms:N-demethyleclanamine;N-desmethyleclanamine;N-desmonomethyleclanamine

Suppliers and Price of N-Desmethyleclanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-Desmethyleclanamine

Chemical Property:

Vapor Pressure:4.9E-08mmHg at 25°C
Boiling Point:442.7°Cat760mmHg
Flash Point:221.6°C
PSA：32.34000
Density:1.24g/cm³
LogP:4.26780
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:314.0952687
Heavy Atom Count:20
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=O)N(C1CCCC1NC)C2=CC(=C(C=C2)Cl)Cl
Isomeric SMILES:CCC(=O)N([C@@H]1CCC[C@H]1NC)C2=CC(=C(C=C2)Cl)Cl

Technology Process of N-Desmethyleclanamine

There total 3 articles about N-Desmethyleclanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69642-67-7
N--N-(3,4-dichlorophenyl)propanamide

: 69642-68-8,116271-40-0
N--N-(3,4-dichlorophenyl)propanamide

Guidance literature:: With acetic acid; zinc; In methanol; for 3h;
DOI:10.1021/jm00142a020

Reference yield:

: 69642-62-2
trans-2-(3,4-dichloroanilino)cyclopentyl hydrogen sulfate

: 69642-68-8,116271-40-0
N--N-(3,4-dichlorophenyl)propanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 159 g / 48 h / 125 °C

2: triethylamine / diethyl ether / 2 h / Ambient temperature

3: 100 percent / Heating

4: zinc, acetic acid / methanol / 3 h

With acetic acid; triethylamine; zinc; In methanol; diethyl ether;
DOI:10.1021/jm00142a020

Reference yield:

: 69642-63-3
trans-N-methyl-N'-(3,4-dichlorophenyl)-1,2-cyclopentanediamine

: 69642-68-8,116271-40-0
N--N-(3,4-dichlorophenyl)propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 2 h / Ambient temperature

2: 100 percent / Heating

3: zinc, acetic acid / methanol / 3 h

With acetic acid; triethylamine; zinc; In methanol; diethyl ether;
DOI:10.1021/jm00142a020