gamma-Resorcylic acid, 3,5-dichloro-4-methyl-

Base Information

• Chemical Name: gamma-Resorcylic acid, 3,5-dichloro-4-methyl-
• CAS No.: 73855-53-5
• Molecular Formula: C₈H₆Cl₂O₄
• Molecular Weight: 237.039
• DSSTox Substance ID: DTXSID30224439
• Nikkaji Number: J85.010A
• Wikidata: Q83103030
• Mol file: 73855-53-5.mol

Synonyms:p-Osellinic acid, 3,5-dichloro-;73855-53-5;gamma-Resorcylic acid, 3,5-dichloro-4-methyl-;3,5-Dichloro-4-methyl-2,6-dihydroxybenzoic acid;Benzoic acid, 3,5-dichloro-2,6-dihydroxy-4-methyl-;C8H5Cl2O4;C8-H5-Cl2-O4;3,5-Dichloro-p-orsellinic acid;DTXSID30224439;LS-143440

Chemical Property of gamma-Resorcylic acid, 3,5-dichloro-4-methyl-

Chemical Property:

• Vapor Pressure: 7.65E-06mmHg at 25°C
• Boiling Point: 361°Cat760mmHg
• Flash Point: 172.1°C
• PSA: 77.76000
• Density: 1.705g/cm³
• LogP: 2.41120
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 235.9643141
• Heavy Atom Count: 14
• Complexity: 219

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=C(C(=C1Cl)O)C(=O)O)O)Cl

Technology Process of gamma-Resorcylic acid, 3,5-dichloro-4-methyl-

There total 6 articles about gamma-Resorcylic acid, 3,5-dichloro-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-(3,5-dichloro-2,6-dihydroxy-4-methylbenzoyl)-5-hydroxy-3-methoxybenzoate (2151-16-8) → 3,5-dichloro-2,6-dihydroxy-4-methyl-benzoic acid (73855-53-5)

Guidance literature:

With sulfuric acid; at 120 ℃;

DOI:10.1007/BF03018946

Reference yield:

2-(3,5-dichloro-2,6-dihydroxy-4-methylbenzoyl)-5-hydroxy-3-methoxybenzoic acid (11029-16-6) → 3,5-dichloro-2,6-dihydroxy-4-methyl-benzoic acid (73855-53-5)

Guidance literature:

With sulfuric acid; at 120 ℃;

DOI:10.1007/BF03018946

Reference yield:

sulfuric acid (7664-93-9) + 2-(3,5-dichloro-2,6-dihydroxy-4-methylbenzoyl)-5-hydroxy-3-methoxybenzoic acid (11029-16-6) → 3-hydroxy-5-methoxybenzoic acid (19520-75-3) + 4,6-dichloro-5-methylresorcinol (63992-61-0) + 3,5-dichloro-2,6-dihydroxy-4-methyl-benzoic acid (73855-53-5)

Guidance literature:

at 125 ℃;

DOI:10.1007/BF03018946

upstream raw materials:

methyl 2-(3,5-dichloro-2,6-dihydroxy-4-methylbenzoyl)-5-hydroxy-3-methoxybenzoate

3,5-dichloro-2,6-dihydroxy-4-methyl-benzoic acid methyl ester

2-(3,5-dichloro-2,6-dihydroxy-4-methylbenzoyl)-5-hydroxy-3-methoxybenzoic acid

sulfuric acid

Downstream raw materials:

3,5-dichloro-2,6-dimethoxy-4-methyl-benzoic acid methyl ester

4,6-dichloro-5-methylresorcinol

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