5-bromo-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde

Base Information

• Chemical Name: 5-bromo-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde
• CAS No.: 22724-20-5
• Molecular Formula: C₅H₃BrN₂O₃
• Molecular Weight: 218.994
• Mol file: 22724-20-5.mol

Synonyms:Orotaldehyde,5-bromo- (8CI); 2,4-Dihydroxy-5-bromopyrimidine-6-carboxaldehyde; 5-Bromoorotaldehyde;NSC 153726

Chemical Property of 5-bromo-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 2.152g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-bromo-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde

There total 2 articles about 5-bromo-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 5-Bromorotaldehyd (22724-20-5)

Guidance literature:

Uracil-4-carbaldehyd-diethylacetal (1), Brom, H2O;

Reference yield:

→ 5-bromo-2,6-dioxo-1,2,3,6-tetrahydro-pyrimidine-4-carbaldehyde (22724-20-5)

Guidance literature:

2,4-Dihydroxy-6-dimethoxymethyl-pyrimidin, Br2, Eisessig;

DOI:10.1021/jm00312a018

Reference yield:

Hippuric Acid (495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2) + 5-bromo-2,6-dioxo-1,2,3,6-tetrahydro-pyrimidine-4-carbaldehyde (22724-20-5) → 5-bromo-6-(5-oxo-2-phenyl-oxazol-4-ylidenemethyl)-1H-pyrimidine-2,4-dione (21328-06-3)

Guidance literature:

With sodium acetate; acetic anhydride; at 90 - 95 ℃;

DOI:10.1021/jm00312a018

Downstream raw materials:

5-bromo-6-(5-oxo-2-phenyl-oxazol-4-ylidenemethyl)-1H-pyrimidine-2,4-dione

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